Catalyst-Free One-Pot Synthesis of Ketene Imines under Ultrasound Irradiation

被引:3
|
作者
Emtiazi, Hamideh [1 ]
Amrollahi, Mohammad A. [1 ]
机构
[1] Yazd Univ, Coll Sci, Dept Chem, Yazd, Iran
关键词
Acetylene esters; Pyridine; 1; 4-dihydro-; Isocyanides; Ketene imine; DIALKYL ACETYLENEDICARBOXYLATES; 3-COMPONENT REACTION; STABLE KETENIMINES; BETA-LACTAMS; ISOCYANIDES; CYCLOADDITION;
D O I
10.1002/hlca.201400002
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
An efficient and simple procedure for the synthesis of ketene imines via a one-pot three-component reaction of cyclohexyl isocyanide, diethyl acetylenedicarboxylate, and 1,4-dihydropyridines under ultrasonic irradiation is described. The remarkable advantages are the simplicity of the experimental procedures, high yields, and short reaction times.
引用
收藏
页码:1422 / 1426
页数:5
相关论文
共 50 条
  • [31] An Efficient Three-component, One-pot Synthesis of Quinazolines under Solvent-free and Catalyst-free Condition
    Bhat, Subrahmanya Ishwar
    Das, U. K.
    Trivedi, Darshak R.
    [J]. JOURNAL OF HETEROCYCLIC CHEMISTRY, 2015, 52 (04) : 1253 - 1259
  • [32] A Catalyst-Free One-Pot Protocol for the Construction of Substituted Isoindolinones under Sustainable Conditions
    Sashidhara, Koneni V.
    Singh, L. Ravithej
    Palnati, Gopala Reddy
    Avula, Srinivasa Rao
    Kant, Ruchir
    [J]. SYNLETT, 2016, 27 (16) : 2384 - 2390
  • [33] Merging catalyst-free synthesis and iodine catalysis: one-pot synthesis of dihydrofuropyrimidines and spirodihydrofuropyrimidine pyrazolones
    Zheng, Ya-Yun
    Feng, Kai-Xiang
    Xia, Ai-Bao
    Liu, Jie
    Tang, Cheng-Ke
    Zhou, Zhan-Yu
    Xu, Dan-Qian
    [J]. RSC ADVANCES, 2019, 9 (17): : 9770 - 9776
  • [34] Catalyst-free one-pot cascade cyclization: An efficient synthesis of isoindolobenzoxazinones and isoindoloquinazolinones derivatives
    Li, Wenzhong
    Wan, Baibai
    Shi, Ran
    Chen, Si
    Li, Jiazhu
    Wang, Fangzhen
    Niu, Hexu
    Xu, Xin-Ming
    Wang, Wei-Li
    [J]. TETRAHEDRON, 2022, 104
  • [35] Catalyst-free one-pot synthesis of quinoline tethered α-amino ketones by multicomponent reactions
    Yadav, Rahul
    Darakshan
    Parvin, Tasneem
    [J]. JOURNAL OF HETEROCYCLIC CHEMISTRY, 2022, 59 (11) : 1935 - 1943
  • [36] Convenient one-pot synthesis of multisubstituted tetrahydropyrimidines via catalyst-free multicomponent reactions
    Zhang, Min
    Jiang, Huanfeng
    Liu, Hailing
    Zhu, Qiuhua
    [J]. ORGANIC LETTERS, 2007, 9 (21) : 4111 - 4113
  • [37] ONE-POT, CATALYST-FREE SYNTHESIS OF SPIROOXINDOLE AND 4H-PYRAN DERIVATIVES
    Ponpandian, Thanasekaran
    Muthusubramanian, Shanmugam
    [J]. SYNTHETIC COMMUNICATIONS, 2014, 44 (06) : 868 - 874
  • [38] GAP chemistry for pyrrolyl coumarin derivatives: a highly efficient one-pot synthesis under catalyst-free conditions
    Wang, Huiyan
    Liu, Xuecheng
    Feng, Xian
    Huang, Zhibin
    Shi, Daqing
    [J]. GREEN CHEMISTRY, 2013, 15 (12) : 3307 - 3311
  • [39] An Efficient Catalyst-Free Protocol for the Synthesis of Quinoxaline Derivatives under Ultrasound Irradiation
    Guo, Wen-Xue
    Jin, Hui-Le
    Chen, Jiu-Xi
    Chen, Fan
    Ding, Jin-Chang
    Wu, Hua-Yue
    [J]. JOURNAL OF THE BRAZILIAN CHEMICAL SOCIETY, 2009, 20 (09) : 1674 - 1679
  • [40] Catalyst-free, one-pot, four-component green synthesis of functionalized 1-(2-fluorophenyl)-1,4-dihydropyridines under ultrasound irradiation
    Shabalala, Nhlanhla
    Maddila, Suresh
    Jonnalagadda, Sreekantha B.
    [J]. NEW JOURNAL OF CHEMISTRY, 2016, 40 (06) : 5107 - 5112