Catalyst-Free One-Pot Synthesis of Ketene Imines under Ultrasound Irradiation

被引：3

作者：

Emtiazi, Hamideh ^{[1
]}

Amrollahi, Mohammad A. ^{[1
]}

机构：

[1] Yazd Univ, Coll Sci, Dept Chem, Yazd, Iran

来源：

HELVETICA CHIMICA ACTA | 2014年 / 97卷 / 10期

关键词：

Acetylene esters; Pyridine; 1; 4-dihydro-; Isocyanides; Ketene imine; DIALKYL ACETYLENEDICARBOXYLATES; 3-COMPONENT REACTION; STABLE KETENIMINES; BETA-LACTAMS; ISOCYANIDES; CYCLOADDITION;

D O I：

10.1002/hlca.201400002

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

An efficient and simple procedure for the synthesis of ketene imines via a one-pot three-component reaction of cyclohexyl isocyanide, diethyl acetylenedicarboxylate, and 1,4-dihydropyridines under ultrasonic irradiation is described. The remarkable advantages are the simplicity of the experimental procedures, high yields, and short reaction times.

引用

页码：1422 / 1426

页数：5

共 50 条

[1] CATALYST-FREE ONE-POT SYNTHESIS OF NOVEL KETENE IMINES
Emtiazi, Hamideh
Amrollahi, Mohammad Ali
[J]. REVUE ROUMAINE DE CHIMIE, 2016, 61 (01) : 47 - +
[2] A one-pot three-component synthesis of novel α-sulfamidophosphonates under ultrasound irradiation and catalyst-free conditions
Belhani, Billel
Berredjem, Malika
Le Borgne, Marc
Bouaziz, Zouhair
Lebreton, Jacques
Aouf, Nour-Eddine
[J]. RSC ADVANCES, 2015, 5 (49) : 39324 - 39329
[3] One-pot and catalyst-free synthesis of pyrroloquinolinediones and quinolinedicarboxylates
Zhang, Xiaofeng
Dhawan, Gagan
Muthengi, Alex
Liu, Shuai
Wang, Wei
Legris, Marc
Zhang, Wei
[J]. GREEN CHEMISTRY, 2017, 19 (16) : 3851 - 3855
[4] Solvent- and catalyst-free synthesis of dihydropyrimidinthiones in one-pot under focused microwave irradiation conditions
Hong Wen Zhan Jin Xian Wang~* Xi Tian Wang Institute of Chemistry
[J]. Chinese Chemical Letters, 2008, (10) : 1183 - 1185
[5] Solvent- and catalyst-free synthesis of dihydropyrimidinthiones in one-pot under focused microwave irradiation conditions
Zhan, Hong Wen
Wang, Jin Xian
Wang, Xi Tian
[J]. CHINESE CHEMICAL LETTERS, 2008, 19 (10) : 1183 - 1185
[6] A One-Pot, Multicomponent Synthesis of Trifluoromethylated Spiropiperidines under Catalyst-Free Conditions
Shi, Wei
Wang, Yang
Zhu, Yingjun
Zhang, Min
Song, Liping
Deng, Hongmei
[J]. SYNTHESIS-STUTTGART, 2016, 48 (20): : 3527 - 3536
[7] Highly efficient one-pot synthesis of trisubstituted imidazoles under catalyst-free conditions
Azizi, Najmadin
Dado, Nairreh
Amiri, Alireza Khajeh
[J]. CANADIAN JOURNAL OF CHEMISTRY, 2012, 90 (02) : 195 - 198
[8] One-Pot Catalyst-Free Synthesis of β- and γ-Hydroxy Sulfides Using Diaryliodonium Salts and Microwave Irradiation
Vaddula, Buchi Reddy
Varma, Rajender S.
Leazer, John
[J]. EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2012, 2012 (35) : 6852 - 6855
[9] A SIMPLE AND CATALYST-FREE ONE-POT SYNTHESIS OF α-AMINOPHOSPHONATES IN POLYETHYLENE GLYCOL
Kumar, M. Anil
Lee, Kap Duk
[J]. PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2012, 187 (08) : 899 - 905
[10] CATALYST-FREE, ONE-POT, EXPEDITIOUS SYNTHESIS OF AMINOALKYLNAPHTHOLS AT ROOM TEMPERATURE
Mukhopadhyay, Chhanda
Rana, Sunil
Butcher, Ray J.
[J]. SYNTHETIC COMMUNICATIONS, 2012, 42 (20) : 3077 - 3088

← 1 2 3 4 5 →