SYNTHESIS OF METHYLENE-BRIDGED RESORCIN[4]ARENE DIMERS

被引：1

作者：

Konishi, Hisatoshi ^{[1
]}

Yokoyama, Rie ^{[1
]}

Hikawa, Katsuhiro ^{[1
]}

Nakada, Takehiro ^{[1
]}

Kobayashi, Kazuhiro ^{[1
]}

Morikawa, Osamu ^{[1
]}

机构：

[1] Tottori Univ, Dept Chem & Biotechnol, Grad Sch Engn, Tottori 680, Japan

来源：

SYNTHETIC COMMUNICATIONS | 2015年 / 45卷 / 05期

关键词：

Host-guest complex; molecular capsule; resorcinarene dimer; CAPSULE FORMATION; INCLUSION; MOLECULES; BEHAVIOR; ARENES; RIM;

D O I：

10.1080/00397911.2011.560988

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Methylene-bridged resorcin[4]arene dimers were synthesized by the Sc(OTf)(3)-catalyzed hydroxymethylation of partially acetylated resorcin[4]arenes, and their preliminary complexation properties with tetraethylammonium ion were examined in CD3OD by H-1 NMR spectroscopy. The dimers adopted a closed capsular conformation in this solvent and bound the guest molecule into their cavity.

引用

页码：615 / 620

页数：6

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