N′-Sulfonyl- and N′-Acylhydrazones of α- and β-Diphenylphosphorylalkanones: Synthesis and Structure

被引:1
|
作者
Uryupin, A. B. [1 ]
Bodrin, G. V. [1 ]
Goryunova, I. B. [1 ]
Goryunov, E. I. [1 ]
Khrustalev, V. N. [2 ,3 ]
Bystrova, N. A. [1 ]
Brel, V. K. [1 ]
Kochetkov, K. A. [1 ,4 ]
机构
[1] Russian Acad Sci, Nesmeyanov Inst Organoelement Cpds, Moscow 119991, Russia
[2] Peoples Friendship Univ Russia, Moscow 117198, Russia
[3] Russian Acad Sci, ND Zelinsky Inst Organ Chem, Moscow 119991, Russia
[4] Mendeleev Russian Univ Chem Technol, Moscow 125047, Russia
关键词
(diarylphosphoryl)alkanones; sulfonyl(acyl)hydrazines; hydrazones; structure; PHOSPHORYLATED KETONE; COMPLEXATION; LANTHANIDES; EXTRACTANT; RECOVERY;
D O I
10.1134/S1070363221040113
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The interaction of saturated acyclic alpha- and beta-(diphenylphosphoryl)alkanones with sulfonyl- and acylhydrazines has led to the corresponding hydrazones in yield up to 90%. Structure of the obtained compounds has been elucidated using the data of single-crystal X-ray diffraction analysis and NMR spectroscopy.
引用
收藏
页码:650 / 656
页数:7
相关论文
共 50 条
  • [41] N-sulfonyl- and N-phosphorylbenzimidoylphosphonates
    Kolotilo, N. V.
    Sinitsa, A. A.
    Rassukanaya, Yu. V.
    Onys'ko, P. P.
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2006, 76 (08) : 1210 - 1218
  • [42] Addition of a carbamoylsilane to N-sulfonylimines: direct synthesis of α-(N-sulfonyl)amino-N-methoxymethyl-N-methylamides
    Liu, Hui
    Guo, Qilin
    Chen, Jianxin
    TETRAHEDRON LETTERS, 2015, 56 (42) : 5747 - 5751
  • [43] Synthesis of N-(coumarin sulfonyl) thiohydantoin and hydantoin derivatives
    Mandour, AH
    Kassem, EM
    AFINIDAD, 2000, 57 (489) : 344 - 348
  • [44] An easy synthesis of aliphatic and aromatic N-sulfonyl aldimines
    Chemla, F
    Hebbe, V
    Normant, JF
    SYNTHESIS-STUTTGART, 2000, (01): : 75 - 77
  • [45] Synthesis of of N-Sulfonyl Pyrrolidines Catalyzed by IPrAuCl/AgOTf
    Yuan, Dongpeng
    Zeng, Ming
    Bai, Chunmei
    Cui, Dongmei
    Zhang, Chen
    CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2014, 34 (06) : 1231 - 1234
  • [46] Anticancer Potential of N-Sulfonyl Noscapinoids: Synthesis and Evaluation
    Nagireddy, Praveen Kumar Reddy
    Kommalapati, Vamsi Krishna
    Krishna, Vagolu Siva
    Sriram, Dharmarajan
    Tangutur, Anjana Devi
    Kantevari, Srinivas
    CHEMISTRYSELECT, 2020, 5 (10): : 2972 - 2980
  • [47] Synthesis of N-organometal substituted sulfonyl derivatives of benzene
    Gordetsov, AS
    Latyaeva, VN
    Levakova, EY
    Zimina, SV
    Cherkasov, VK
    Kulagina, NV
    Kozina, AP
    ZHURNAL OBSHCHEI KHIMII, 1997, 67 (05): : 833 - 837
  • [48] Synthesis N-ethylpiperazinyl sulfonyl group incorporated benzamides
    Patel, NB
    Rathod, RD
    INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY, 2005, 15 (02) : 201 - 202
  • [49] Reactions of N-acylhydrazones with thionyl chloride
    Kotali, A
    Lafazanis, IS
    ARKIVOC, 2003, : 91 - 94
  • [50] Strecker reactions of chiral N-acylhydrazones
    Ding, Hui
    Friestad, Gregory K.
    HETEROCYCLES, 2006, 70 : 185 - +