Synthesis and characterization of 6-(p-chlorobenzoyl)-5,7,12,14-tetramethyl-benzo[b]-1,4,8,11-tetraazacyclo[14]tetradecinato(2-)nickel(II)

被引：1

作者：

Kim, DI

Lim, JW

Na, HG

Choi, JH

Park, YC ^{[1
]}

Yoshioka, D

Mikuriya, M

机构：

[1] Kyungpook Natl Univ, Dept Chem, Taegu 702701, South Korea

[2] Daejin Univ, Dept Chem, Pochon 487800, South Korea

[3] Andong Natl Univ, Dept Chem, Andong 760749, South Korea

[4] Kwansei Gakuin Univ, Sch Sci & Technol, Dept Chem, Sanda 6691337, Japan

来源：

INORGANICA CHIMICA ACTA | 2005年 / 358卷 / 02期

基金：

新加坡国家研究基金会;

关键词：

crystal structures; nickel(II) complexes; macrocyclic ligands;

D O I：

10.1016/j.ica.2004.07.041

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A nickel(II) complex with 6-(p-chlorobenzoyl)-5,7,12,14-tetramethyl-benzo[b]-1,4,8,11-tetraazacyclo[14]tetradecine was synthesized and characterized by measurements of NMR, IR and an electronic spectra. The X-ray crystal structure shows that the coordination geometry around the Ni atom is a square planar with the unsymmetrical tetraaza[14]annulene. (C) 2004 Elsevier B.V. All rights reserved.

引用

页码：419 / 422

页数：4

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