Synthesis and characterization of 6-(p-chlorobenzoyl)-5,7,12,14-tetramethyl-benzo[b]-1,4,8,11-tetraazacyclo[14]tetradecinato(2-)nickel(II)

被引：1
|
作者：
Kim, DI
Lim, JW
Na, HG
Choi, JH
Park, YC [1 ]
Yoshioka, D
Mikuriya, M
机构：
[1] Kyungpook Natl Univ, Dept Chem, Taegu 702701, South Korea
[2] Daejin Univ, Dept Chem, Pochon 487800, South Korea
[3] Andong Natl Univ, Dept Chem, Andong 760749, South Korea
[4] Kwansei Gakuin Univ, Sch Sci & Technol, Dept Chem, Sanda 6691337, Japan
来源：
INORGANICA CHIMICA ACTA | 2005年 / 358卷 / 02期
基金：
新加坡国家研究基金会;
关键词：
crystal structures; nickel(II) complexes; macrocyclic ligands;
D O I：
10.1016/j.ica.2004.07.041
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A nickel(II) complex with 6-(p-chlorobenzoyl)-5,7,12,14-tetramethyl-benzo[b]-1,4,8,11-tetraazacyclo[14]tetradecine was synthesized and characterized by measurements of NMR, IR and an electronic spectra. The X-ray crystal structure shows that the coordination geometry around the Ni atom is a square planar with the unsymmetrical tetraaza[14]annulene. (C) 2004 Elsevier B.V. All rights reserved.
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页码：419 / 422
页数：4
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