Solvothermal synthesis and magnetic properties of 3D flower-like NiHPO3•H2O superstructures

被引：5
|
作者：
Sun, Xiujuan [1 ]
Xing, Yan [1 ]
Liu, Xianchun [1 ]
Liu, Bo [1 ]
Hou, Suying [1 ]
机构：
[1] NE Normal Univ, Coll Chem, Changchun 130024, Peoples R China
来源：
DALTON TRANSACTIONS | 2010年 / 39卷 / 08期
关键词：
HYDROTHERMAL SYNTHESIS; LARGE-SCALE; PHOSPHITE; FABRICATION; NANOCRYSTALS; DIFFRACTION; ARRAYS; CO;
D O I：
10.1039/b919177a
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A self-assembled three-dimensional (3D) flower-like NiHPO3 center dot H2O micro/nanocomposite structure has been successfully synthesized for the first time by a simple solvothermal method, employing Na6P6O18 as the phosphor source without the assistance of any template or surfactant. The as-obtained product was characterized by X-ray powder diffraction, scanning electron microscopy and transmission electron microscopy. The formation mechanism was proposed based on the evolution of this morphology as a function of solvothermal time. Some factors influencing the morphology of the NiHPO3 center dot H2O flower-like micro/nanocomposite structures were systematically investigated. The magnetic measurements demonstrated that the flower-like 3D superstructures exhibit ferromagnetic property.
引用
收藏
页码：1985 / 1988
页数：4
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