Hypervalent iodine in synthesis 91: a mild and efficient method for the halogenation of 6-methyluracil derivatives

被引：0
|
作者：
Cheng, DP
Chen, ZC
Zheng, QG
机构：
[1] Zhejiang Univ, Dept Chem, Hangzhou 310028, Peoples R China
[2] Aston Univ, Sch Life & Hlth Sci, Birmingham B4 7ET, W Midlands, England
来源：
JOURNAL OF CHEMICAL RESEARCH | 2002年 / 12期
关键词：
hypervalent iodine; halogenation; 6-methyluracil derivatives;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The combined reagent of iodobenzene diacetate (or polymer-supported iodobenzene diacetate) with iodine or bromine was used as an effective halogenative agent of 6-methyluracil derivatives to the corresponding 5-halo-6-methyluracil derivatives at room temperature with high yields.
引用
收藏
页码：624 / 625
页数：2
相关论文
共 50 条
  • [21] REACTION OF SULFAMIDE WITH DIKETENE - SYNTHESIS OF AN S-DIOXO ANALOG OF 6-METHYLURACIL
    DIE, R
    DIEZ, J
    STUD, M
    MADRONER.R
    GARCIAMU.G
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 1972, 9 (04) : 973 - &
  • [22] Efficient synthesis of quinoxalines with hypervalent iodine as a catalyst
    Chen, Chung-Yu
    Hu, Wan-Ping
    Liu, Mei-Chun
    Yan, Pi-Cheng
    Wang, Jeh-Jeng
    Chung, Mei-Ing
    TETRAHEDRON, 2013, 69 (46) : 9735 - 9741
  • [23] BIOLOGICAL-ACTIVITY OF 6-METHYLURACIL (6-MU) IN COMPARISON WITH PESTICIDE-TYPE DERIVATIVES
    POZSAR, BI
    ACTA AGRONOMICA ACADEMIAE SCIENTIARUM HUNGARICAE, 1979, 28 (1-2): : 170 - 184
  • [24] 1,3-DI(3-DIMETHOXYPHOSPHORYLPROPYL) DERIVATIVES OF URACIL AND 6-METHYLURACIL - SYNTHESIS AND BIOLOGICAL-ACTIVITY
    KOVALEV, GV
    RAKHIMOV, AI
    OZEROV, AA
    PETROV, VI
    SPASOV, AA
    VASILYEV, PM
    KOVALEV, SG
    NOVIKOV, MS
    ROZENBLIT, AB
    GOLENDER, VY
    KOFMAN, AM
    KHIMIKO-FARMATSEVTICHESKII ZHURNAL, 1990, 24 (06): : 25 - 27
  • [25] Inhibiting effect of 6-methyluracil derivatives on the free -radical oxidation of 1,4-dioxane
    L. R. Yakupova
    A. V. Ivanova
    R. L. Safiullin
    A. R. Gimadieva
    Yu. N. Chernyshenko
    A. G. Mustafin
    I. B. Abdrakhmanov
    Russian Chemical Bulletin, 2010, 59 : 517 - 521
  • [26] Efficient modification of peroxydisulfate oxidation reactions of nitrogen-containing heterocycles 6-methyluracil and pyridine
    Gimadieva, Alfiya R.
    Khazimullina, Yuliya Z.
    Gilimkhanova, Aigiza A.
    Mustafin, Akhat G.
    BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY, 2024, 20 : 2599 - 2607
  • [27] Synthesis of 5-[2-(phenoxy)ethyl] derivatives of 6-methyluracil, 2-thio-6-methyluracil, and 2-amino-6-methylpyrimidin-4(3H)-one
    Novikov, MS
    Ozerov, AA
    Sim, OG
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 2005, (08): : 1213 - 1217
  • [28] Hypervalent iodine-mediated efficient synthesis of imidazoles
    Das, Biswanath
    Srinivas, Yallamalla
    Holla, Harish
    Krishnaiah, Maddeboina
    Narender, Ravirala
    CHEMISTRY LETTERS, 2007, 36 (10) : 1270 - 1271
  • [29] An efficient method for the synthesis of naphthoquinoline derivatives catalyzed by iodine
    Wang, Wei
    Lu, Lian
    Wang, Xiang-Shan
    HETEROCYCLIC COMMUNICATIONS, 2012, 18 (01) : 17 - 21
  • [30] Iodine-Catalyzed Mild and Efficient Method for the Synthesis of Chalcones
    Sashidhara, Koneni V.
    Rosaiah, Jammikuntla N.
    Kumar, Abdhesh
    SYNTHETIC COMMUNICATIONS, 2009, 39 (13) : 2288 - 2296
12345