Template synthesis and structure of Ni(II), Cu(II), Co(II), and Co(III) hexaazamacrocyclic compounds based on S-alkylisothiosemicarbazide

被引：0
|
作者：
Gredinaru, DI [1 ]
Gerbeleu, NV
Arion, VB
Simonov, YA
Popovich, MA
Bourosh, PN
机构：
[1] Moldavian Acad Sci, Inst Chem, Chisinau, Moldova
[2] Moldavian Acad Sci, Inst Appl Phys, Chisinau, Moldova
来源：
RUSSIAN JOURNAL OF INORGANIC CHEMISTRY | 2000年 / 45卷 / 04期
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D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
New Cu(II), Co(II), Co(III), and Ni(II) hexaazamacrocyclic complexes based on S-alkylisothiosemicarbazide and beta-dicarbonyl compounds were synthesized and characterized by IR, H-1 NMR, and C-13 NMR spectroscopy, mass spectrometry, magnetochemistry, EPR, and thermogravimetry. An X-ray diffraction study of [3,9-bis(propylthio)-13-nitro-1,2,4,8,10,11-hexaazacyclotetradeca-2,4,6,9,10,13-hexaenato(2-)-N-1,N-4,N-8,N-11]copper(II) confirmed the square-planar structure of the compounds in question.
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页码：533 / 543
页数：11
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