Crystal structure of β form of [PtEnCl2]

被引：0
|
作者：
Koz'min, PA [1 ]
Surazhskaya, MD [1 ]
Fedotova, TN [1 ]
Kuznetsova, GN [1 ]
Minacheva, LK [1 ]
Baranovskii, IB [1 ]
机构：
[1] NS Kurnakov Gen & Inorgan Chem Inst, Moscow 117907, Russia
来源：
RUSSIAN JOURNAL OF INORGANIC CHEMISTRY | 2000年 / 45卷 / 07期
关键词：
D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Triclinic crystals of [PtEnCl(2)], prepared by the redox reaction of [EnPt(mu-NHCOCH3)(2)PtEn](NO3)(2) with chlorine water, are structurally studied by X-ray diffraction. The unit cell parameters are a = 6.542(2) rq, b = 6.909(7) Angstrom, c = 8.046(3) Angstrom, alpha = 83.32(6)degrees, beta = 68.52(3)degrees, gamma = 68.63(6)degrees, V = 315.3(4) Angstrom(3), Z = 2, space group P (1) over bar, R-hkl = 0.026. In the crystal, the [PtEnCl(2)] complexes form columns parallel to the [010] direction. The platinum atoms are located in a line close to the gamma axis.
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页码：1036 / 1038
页数：3
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