The crystal structure of 17-(bromoethynyl)-17-hydroxy-10, 13-dimethyl-1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-3H-cyclopenta[a]phenanthren-3-one, C21H27BrO2

被引：0

作者：

Ji, Xiao-Liang ^{[1
]}

Xie, Feng ^{[1
]}

Li, Yi-Biao ^{[1
]}

机构：

[1] Wuyi Univ, Sch Biotechnol & Hlth Sci, Jiangmen 529020, Peoples R China

来源：

ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2022年 / 237卷 / 04期

关键词：

2059794;

D O I：

10.1515/ncrs-2022-0165

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

C21H27BrO2, monoclinic, P2(1) (no. 4), a = 6.6220(14) angstrom, b = 11.7640(2) angstrom, c = 11.8485(2) angstrom, beta = 95.0757(19)degrees V = 919.39(3) angstrom(3), Z = 2, R ( gt )(F) = 0.0264, wR ( ref )(F (2)) = 0.0695, T = 150 K, Flack-parameter = 0.007(13).

引用

页码：655 / 657

页数：3

共 50 条

[41] Crystal structure of (E)-7-hydroxy-2-((6-methoxypyridin-2-yl)methylene)-3,4-dihydronaphthalen-1(2H)-one, C17H15NO3
Liang, Lun-Hai
Zhao, Feng-Lan
Meng, Qing-Guo
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2021, 236 (05): : 1125 - 1127
[42] anti-2,2,3,3,6,6,7,7,10,10,11,11,14,14,15,15-Hexadecamethy1-2,3,6,7,10,11,- 14,15-octasilapentacyclo[1 0.4.2.2(4'9).0(5'8).0(13'16)]icosa-1 (1 7),4,8,12(18),13(1 6),19-hexaene
Toma, Yuki
Otsuka, Kyohei
Kyushin, Soichiro
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O341 - +
[43] Synthesis and crystal structure of 1-((3R,10S,13R,17S)-3-((4-methoxyphenyl)amino)-10,13-dimethylhexadecahydro-1H-cyclopenta[α]-phenanthren-17-yl)ethan-1-one, C28H41NO2
Zhang, Wen-Wen
Ye, Jiang-Hai
Huang, Hua
Zou, Juan
He, Kang
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2023, 238 (02): : 189 - 191
[44] (+/-)-(3aR(*),6S(*),7S(*),14aR(*))-2,3,3a,7,8,9,10,11,12,13,14,14a-dodecahydro-1H,6H-3a,6-epoxy-7,14a-methanocyclopentacyclo-tridecen-15-one
Harmata, M
Elomari, S
Barnes, CL
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1996, 52 : 1209 - 1211
[45] SYNTHESIS OF THE FIRST 3,6,9,12,15,18-HEXA-SUBSTITUTED-1,2,4,5,7,8,10,11,13,14,16,17-DODECADEHYDRO[18]ANNULENES WITH D(6H)-SYMMETRY
KUWATANI, Y
WATANABE, N
UEDA, I
TETRAHEDRON LETTERS, 1995, 36 (01) : 119 - 122
[46] Crystal structure of 6,8,14,16-tetraamino-2,3,4,10,11,12-hexathiatricyclo-[11.3.1.15,9]octadeca-5,7,9 (18),13(17), 14,16-hexaen-dimethylformamide (1/2), [C6H2(NH2)2(S3)]2•2DMF
Getzschmann, J
Rademacher, O
Doert, T
Böttcher, P
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 1999, 214 (02): : 255 - 256
[47] CRYSTAL STRUCTURE OF 7,15,17,19-TETRAETHOXY-2,3,4,5,10,11,12,13-OCTATHIATRICYCLO[12,2,2,26,9]EICOSA-6,8,14,16,17,19-HEXAENE, A SULPHUR ANALOGUE OF PARACYCLOPHANES
RICCI, JS
BERNAL, I
JOURNAL OF THE CHEMICAL SOCIETY B-PHYSICAL ORGANIC, 1971, (10): : 1928 - &
[48] Synthesis and crystal structure of-(3S,10S,13S,17S)-N-(2-methoxyphenyl)-10,13-dimethyl-17-((R)-1-(phenylamino)ethyl)hexadecahydro-1H-cyclopenta[α]phenanthren-3-amine, C34H48N2O
Li, Lu-Lu
Wei, Peng
Ye, Jiang-Hai
Zou, Juan
He, Kang
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2025, 240 (02): : 195 - 197
[49] (1 ' S, 12 ' R, 13 ' S, 17 ' S)-15 ',15 '-Dimethyl-1,2-dihydro-11 ',14 ',16 ',18 '-tetraoxa-7 '-azaspiro[indole-3,8 '-pentacyclo-[10.6.0.0(2,9).0(3,7).0(13,17)]octadecane]-2,10 '-dione
Sabari, V.
Ponnusamy, R.
Prasanna, R.
Raghunathan, R.
Aravindhan, S.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O466 - +
[50] 2,2,7,7,12,12,17,17-Octamethyl21,22,23,24-tetrathia-2,7,12,17- tetragermapentacyclo[16.2.1.1(3,6).1(8,1)1.1(13,16)]tetracosa- 3,5,8,10,13,15,18,20-octaene
Carel, Guillaume
Mallettadeira, Sonia
Rima, Ghassoub
Madec, David
Castel, Annie
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : M37 - +

← 1 2 3 4 5 →