Microwave-assisted acylation of amines, alcohols, and phenols by the use of solid-supported reagents (SSRs)

被引:37
|
作者
Petricci, E [1 ]
Mugnaini, C [1 ]
Radi, M [1 ]
Corelli, F [1 ]
Botta, M [1 ]
机构
[1] Univ Siena, Dipartimento Farmaco Chim Tecnol, I-53100 Siena, Italy
来源
JOURNAL OF ORGANIC CHEMISTRY | 2004年 / 69卷 / 23期
关键词
D O I
10.1021/jo048837q
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A microwave-assisted synthesis of solid-supported reagents for the acylation of amines has been developed, and the same methodology has been successfully applied to the preparation of acylating agents anchored on different solid supports. Similarly, alcohols, phenols, and thiophenols have been easily acylated using these reagents under microwave irradiation.
引用
收藏
页码:7880 / 7887
页数:8
相关论文
共 50 条
  • [11] Solid-supported reagents in organic synthesis using microwave irradiation
    Department of Chemistry, School of Science, Alzahra University, PO Box 1993891176, Vanak, Tehran, Iran
    Heravi, M. M. (mmh1331@yahoo.com), 1600, Bentham Science Publishers (17):
  • [12] Two efficient N-acylation methods of weakly acidic heterocyclic amines mediated by solid-supported reagents.
    Kim, K
    Le, K
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1999, 218 : U120 - U120
  • [13] Microwave-assisted NiCl2 promoted acylation of alcohols
    Constantinou-Kokotou, V
    Peristeraki, A
    SYNTHETIC COMMUNICATIONS, 2004, 34 (22) : 4227 - 4232
  • [14] Solid-supported reagents, catalysts and their use to solution phase synthesis
    Zhang, Liang
    Liu, Gang
    CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2006, 26 (07) : 885 - 898
  • [15] Novel synthetic approach in microwave-assisted solid-supported oxidations using 'in situ' generated molecular oxygen
    Gershonov, Eytan
    Katz, Esther
    Karton, Yishai
    Zafrani, Yossi
    TETRAHEDRON, 2007, 63 (18) : 3762 - 3767
  • [16] MICROWAVE-ASSISTED ESTERIFICATION OF PHOSPHINIC ACIDS BY ALCOHOLS, PHENOLS, AND ALKYL HALOGENIDES
    Keglevich, Gyorgy
    Nora Zs. Kiss
    Balint, Erika
    Jablonkai, Erzsebet
    Gruen, Alajos
    Matyas Milen
    David Frigyes
    Istvan Greiner
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2011, 186 (04) : 802 - 803
  • [17] Highly Practical Aqueous Phase Acylation of Phenols, Amines and Alcohols Employing New Green Acylation Reagents Derived From DBU
    Thangalipalli, Swathi
    Bandalla, Siddarama Goud
    Gavinolla, Vijayalaxmi
    Kairoju, Srikanth
    Panduga, Ramaraju
    Neella, Chandra Kiran
    CHEMISTRYSELECT, 2024, 9 (08):
  • [18] Solid-supported tert-alkoxycarbonylation reagents for anchoring of amines during solid phase organic synthesis
    Hernandez, AS
    Hodges, JC
    JOURNAL OF ORGANIC CHEMISTRY, 1997, 62 (10): : 3153 - 3157
  • [19] Solid-Supported tert-Alkoxycarbonylation Reagents for Anchoring of Amines during Solid Phase Organic Synthesis
    Hernandez, A. S.
    Hodges, J. C.
    Journal of Organic Chemistry, 62 (10):
  • [20] Microwave-assisted preparation of dialkylimidazolium tetrachloroaluminates and their use as catalysts in the solvent-free tetrahydropyranylation of alcohols and phenols
    Namboodiri, VV
    Varma, RS
    CHEMICAL COMMUNICATIONS, 2002, (04) : 342 - 343