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Preparation of TiC/W core-shell structured powders by one-step activation and chemical reduction process
被引:21
|作者:
Ding, Xiao-Yu
[1
]
Luo, Lai-Ma
[1
,3
]
Huang, Li-Mei
[1
]
Luo, Guang-Nan
[2
]
Zhu, Xiao-Yong
[1
,3
]
Cheng, Ji-Gui
[1
,3
]
Wu, Yu-Cheng
[1
,3
]
机构:
[1] Hefei Univ Technol, Coll Mat Sci & Engn, Hefei 230009, Peoples R China
[2] Chinese Acad Sci, Inst Plasma Phys, Hefei 230031, Peoples R China
[3] Engn Res Ctr Powder Met Anhui Prov, Hefei 230009, Peoples R China
基金:
中国国家自然科学基金;
关键词:
One-step activation;
Chemical reduction;
TiC/W;
Core-shell;
COMPOSITES;
TUNGSTEN;
NANOPARTICLES;
ENHANCEMENT;
EVOLUTION;
STRENGTH;
ALLOYS;
D O I:
10.1016/j.jallcom.2014.08.242
中图分类号:
O64 [物理化学(理论化学)、化学物理学];
学科分类号:
070304 ;
081704 ;
摘要:
In the present study, one-step activation and chemical reduction process as a novel wet-chemical route was performed for the preparation of TiC/W core-shell structured ultra-fine powders. The XRD, FE-SEM, TEM and EDS results demonstrated that the as-synthesized powders are of high purity and uniform with a diameter of approximately 500 nm. It is also found that the TiC nanoparticles were well-encapsulated by W shells. Such a unique process suggests a new method for preparing X/W (X refers the water-insoluble nanoparticles) core-shell nanoparticles with different cores. (C) 2014 Elsevier B.V. All rights reserved.
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页码:704 / 708
页数:5
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