Preparation of TiC/W core-shell structured powders by one-step activation and chemical reduction process

被引:21
|
作者
Ding, Xiao-Yu [1 ]
Luo, Lai-Ma [1 ,3 ]
Huang, Li-Mei [1 ]
Luo, Guang-Nan [2 ]
Zhu, Xiao-Yong [1 ,3 ]
Cheng, Ji-Gui [1 ,3 ]
Wu, Yu-Cheng [1 ,3 ]
机构
[1] Hefei Univ Technol, Coll Mat Sci & Engn, Hefei 230009, Peoples R China
[2] Chinese Acad Sci, Inst Plasma Phys, Hefei 230031, Peoples R China
[3] Engn Res Ctr Powder Met Anhui Prov, Hefei 230009, Peoples R China
基金
中国国家自然科学基金;
关键词
One-step activation; Chemical reduction; TiC/W; Core-shell; COMPOSITES; TUNGSTEN; NANOPARTICLES; ENHANCEMENT; EVOLUTION; STRENGTH; ALLOYS;
D O I
10.1016/j.jallcom.2014.08.242
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
In the present study, one-step activation and chemical reduction process as a novel wet-chemical route was performed for the preparation of TiC/W core-shell structured ultra-fine powders. The XRD, FE-SEM, TEM and EDS results demonstrated that the as-synthesized powders are of high purity and uniform with a diameter of approximately 500 nm. It is also found that the TiC nanoparticles were well-encapsulated by W shells. Such a unique process suggests a new method for preparing X/W (X refers the water-insoluble nanoparticles) core-shell nanoparticles with different cores. (C) 2014 Elsevier B.V. All rights reserved.
引用
收藏
页码:704 / 708
页数:5
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