catena-Poly[[[aqua[(2-hydroxyphenyl)acetato-κ2O,O′]lead(II)]-μ3-[(2-hydroxyphenyl)acetato-κ4O:O,O′:O′]] monohydrate]

被引：2
|
作者：
Xiao, Jun-Xia [1 ]
Wu, Xian-Ge [1 ]
Qin, Liang [1 ]
机构：
[1] Zhaoqing Univ, Sch Chem & Chem Engn, Zhaoqing 526061, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷
关键词：
Data-to-parameter ratio = 13.5; Mean σ(C-C) = 0.009 Å; R factor = 0.036; Single-crystal X-ray study; T = 293 K; WR factor = 0.084;
D O I：
10.1107/S1600536810004162
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title complex, {[Pb(C8H7O3)(2)(H2O)]center dot H2O}(n), the Pb-II atom is seven-coordinated by six carboxylate O atoms from four different 2-hydroxyphenylacetate (2-dph) ligands and one water molecule, displaying a hemidirected irregular geometry, with the empty side of the metal ion capped by a benzene ring forming a Pb center dot center dot center dot pi contact [Pb center dot center dot center dot centroid distance = 3.342 (2) angstrom]. One 2-dph ligand functions in a bridging mode and connects Pb ions into a linear chain. The crystal packing is governed by intra-and intermolecular O-H center dot center dot center dot O hydrogen bonds.
引用
收藏
页码：M273 / U3298
页数：11
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