A new method for synthesis of a HMFI/SiC composite

被引:1
|
作者
Dedov, Alexey G. [1 ]
Karavaev, Alexander A. [1 ,2 ]
Loktev, Alexey S. [1 ,2 ,3 ]
Mitinenko, Alexey S. [1 ]
Cherednichenko, Kirill A. [1 ]
Moiseev, Ilya I. [1 ]
机构
[1] Gubkin Univ, Natl Univ Oil & Gas, 65 Leninsky Pr, Moscow 119991, Russia
[2] Russian Acad Sci, AV Topchiev Inst Petrochem Synth, 29 Leninsky Pr, Moscow 119991, Russia
[3] Russian Acad Sci, NS Kurnakov Inst Gen & Inorgan Chem, 31 Leninsky Pr, Moscow 119991, Russia
基金
俄罗斯基础研究基金会;
关键词
HMFI; SiC composite; Hydrothermal-microwave synthesis; Porous materials; Zeolites; SIC FOAM SUPPORT; ZSM-5; COATINGS; ZEOLITE CATALYSTS; METHANOL; BETA; OLEFINS; GREEN;
D O I
10.1016/j.matlet.2021.129497
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
HMFI/SiC composites show considerable potential for applications in heterogeneous catalysis due to the combination of the high catalytic performance of HMFI zeolites and the high thermal conductivity, mechanical strength, high-temperature resistance, and good chemical stability of SiC. Herein, we report for the first time the fast synthesis of HMFI/SiC composites directly in proton form under microwave irra-diation without the addition of seed crystals. The preferable conditions for producing HMFI/SiC directly in proton form are 3 hat 190-200 degrees C. The structure and properties of the synthesized HMFI/SiC were deter-mined by X-ray diffraction, scanning electron microscopy, low-temperature adsorption-desorption of nitrogen and temperature-programmed desorption of ammonia. (c) 2021 Elsevier B.V. All rights reserved.
引用
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页数:3
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