Synthesis and Characterization of Magnesium Oxybromide Mg2(OH)3Br•4 H2O

被引:0
|
作者
Lauermannova, Anna-Marie [1 ]
Lojka, Michal [1 ]
Antoncik, Filip [1 ]
Jankovsky, Ondrej [1 ]
机构
[1] Univ Chem & Technol, Dept Inorgan Chem, Fac Chem Technol, Tech 5, Prague 16628 6, Czech Republic
关键词
CEMENT;
D O I
10.1063/5.0033865
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Magnesium oxybromides are analogue substances to magnesium oxychlorides, commonly known as Sorel cements. In this contribution, we prepared and characterized pure Mg-2(OH)(3)Br center dot 4H(2)O. The phase composition was evaluated by X-ray diffraction. The chemical composition was analyzed using X-ray fluorescence and energy dispersive spectroscopy. Also, scanning electron microscopy and transmission electron microscopy was used to analyse the microstructure. In addition, thermal stability was tested using simultaneous thermal analysis.
引用
收藏
页数:7
相关论文
共 50 条
  • [31] Theoretical study on the difference of OH vibrational spectra between OH-(H2O)3 and OH-(H2O)4
    Morita, Masato
    Takahashi, Kaito
    PHYSICAL CHEMISTRY CHEMICAL PHYSICS, 2012, 14 (08) : 2797 - 2808
  • [32] Synthesis and Characterization of [M2(OH)2(C4O4)2(H2O)4]•2H2O (M = Al or Ga)
    Halis, Selda
    Reinsch, Helge
    Stock, Norbert
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2016, 642 (23): : 1340 - 1344
  • [33] Synthesis and Crystal Structure of BaZn(OH)4 H2O
    Z Anorg Allg Chem, 1 (21):
  • [34] EXTREMELY ASYMMETRICALLY BOUND WATER-MOLECULES - CRYSTAL-STRUCTURES OF SR(OH)CL.4 H2O, SR(OH)BR.4 H2O, AND BA(OH)I.4 H2O
    KELLERSOHN, T
    BECKENKAMP, K
    LUTZ, HD
    ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 1991, 46 (10): : 1279 - 1286
  • [35] Synthesis and crystal structure of BaZn(OH)4•H2O
    Stahl, R
    Jacobs, H
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1998, 624 (01): : 21 - 24
  • [36] ABINITIO STUDIES OF NEGATIVE-ION MOLECULE(S) CLUSTERS PRESENT IN THE ATMOSPHERE .2. OH-(H2O)0, OH-(H2O)2, OH-(H2O)3, OH-(H2O)4
    SAPSE, AM
    OSORIO, L
    SNYDER, G
    INTERNATIONAL JOURNAL OF QUANTUM CHEMISTRY, 1984, 26 (02) : 223 - 230
  • [37] Interaction Energy and the Shift in OH Stretch Frequency on Hydrogen Bonding for the H2O→H2O, CH3OH→H2O, and H2O→CH3OH dimers
    Campen, Richard Kramer
    Kubicki, James D.
    JOURNAL OF COMPUTATIONAL CHEMISTRY, 2010, 31 (05) : 963 - 972
  • [38] Raman microscopy of haidingerite Ca(AsO3OH)•H2O and brassite Mg(AsO3OH)• 4H2O
    Frost, Ray L.
    Bahfenne, Silmarilly
    Cejka, Jiri
    Sejkora, Jiri
    Palmer, Sara J.
    Skoda, Radek
    JOURNAL OF RAMAN SPECTROSCOPY, 2010, 41 (06) : 690 - 693
  • [39] THE CRYSTAL STRUCTURE OF ARTINITE, MG2(OH)2CO3.3H2O
    DEWOLFF, PM
    ACTA CRYSTALLOGRAPHICA, 1952, 5 (02): : 286 - 287
  • [40] Structural characterization of lead (II) oxybromide Pb3O2Br2
    Moscow State Univ, Moscow, Russia
    Mater Res Bull, 6 (717-722):