FTIR, 1H and 13C NMR spectra of 1:1 complexes of 1-piperidineacetic acid and N-methylpiperidine betaine with mineral acids

被引：22

作者：

Dega-Szafran, Z ^{[1
]}

Dulewicz, E ^{[1
]}

Petryna, M ^{[1
]}

机构：

[1] Adam Mickiewicz Univ Poznan, Fac Chem, PL-60780 Poznan, Poland

来源：

JOURNAL OF MOLECULAR STRUCTURE | 2003年 / 651卷

关键词：

1-piperidineacetic acid; N-methylpiperidine betaine; FTIR; H-1 and C-13 NMR;

D O I：

10.1016/S0022-2860(02)00689-0

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Syntheses of 1:1 complexes of 1-piperidineacetic acid (PAA) and N-methylpiperidine betaine (MPH) with HCl, HBr, HI, HNO3, HClO4, HBF4 and their H-1 and C-13 NMR spectra in D2O and powdered FTIR spectra are described. The difference between the spectra of theses two series of complexes are discussed and analysed in order to determine the effect of the N-H replacement by N-CH3 group. (C) 2003 Elsevier Science B.V. All rights reserved.

引用

页码：635 / 644

页数：10

共 50 条

[11] 1H and 13C NMR spectra of some drimanic sesquiterpenoids
Panasenko, AA
Gorincioi, EC
Aricu, AN
Barcari, EA
Deleanu, K
Vlad, PF
RUSSIAN CHEMICAL BULLETIN, 2004, 53 (12) : 2700 - 2705
[12] Complete assignment of 1H and 13C NMR spectra of vinflunine
Ribet, JP
Zalavari, P
Fahy, J
Duflos, A
Beltran, T
MAGNETIC RESONANCE IN CHEMISTRY, 2001, 39 (01) : 43 - 48
[13] 1H and 13C NMR spectra for a series of arylmaleamic acids, arylmaleimides, arylsuccinamic acids and arylsuccinimides
Trujillo-Ferrara, J
Santillan, R
Beltrán, HI
Farfán, N
Höpfl, H
MAGNETIC RESONANCE IN CHEMISTRY, 1999, 37 (09) : 682 - 686
[14] Complexes of diphenylarsinic acid and phenylarsonic acid with thiols:: a 1H and 13C NMR study
Nakayama, T
Isobe, T
Nakamiya, K
Edmonds, JS
Shibata, Y
Morita, M
MAGNETIC RESONANCE IN CHEMISTRY, 2005, 43 (07) : 543 - 550
[15] On the use of 1H and 13C 1D NMR spectra as QSPR descriptors
Willighagen, EL
Denissen, HMGW
Wehrens, R
Buydens, LMC
JOURNAL OF CHEMICAL INFORMATION AND MODELING, 2006, 46 (02) : 487 - 494
[16] Predicting the 1H and 13C NMR spectra of paramagnetic Ru(III) complexes by DFT
Rastrelli, Federico
Bagno, Alessandro
MAGNETIC RESONANCE IN CHEMISTRY, 2010, 48 : S132 - S141
[17] 1H and 13C NMR spectra of Strychnos alkaloids: Selected NMR updates
Semenov, Valentin A.
Samultsev, Dmitry O.
Krivdin, Leonid B.
INTERNATIONAL JOURNAL OF QUANTUM CHEMISTRY, 2020, 120 (19)
[18] Complete 1H and 13C NMR assignments of stephalic acid
Burgueño-Tapia, E
Hernández, LR
Joseph-Nathan, P
Salmón, M
MAGNETIC RESONANCE IN CHEMISTRY, 1999, 37 (06) : 430 - 432
[19] Reassignment of the 1H NMR spectrum of fusidic acid and total assignment of 1H and 13C NMR spectra of some selected fusidane derivatives
Rastrup-Andersen, N
Duvold, T
MAGNETIC RESONANCE IN CHEMISTRY, 2002, 40 (07) : 471 - 473
[20] Experimental and calculated 1H, 13C, 15N NMR spectra of famotidine
Baranska, M
Czarniecki, K
Proniewicz, LM
JOURNAL OF MOLECULAR STRUCTURE, 2001, 563 : 347 - 351

← 1 2 3 4 5 →