Analysis of Volatile Compounds in the Pericarp of Zanthoxylum bungeanum Maxim. by Ultrasonic Nebulization Extraction Coupled with Headspace Single-Drop Microextraction and GC-MS

被引：29
|
作者：
Wang, Lu [1 ]
Wang, Ziming [1 ]
Li, Xueyuan [1 ]
Zhang, Huihui [1 ]
Zhou, Xin [2 ]
Zhang, Hanqi [1 ]
机构：
[1] Jilin Univ, Coll Chem, Changchun 130012, Peoples R China
[2] Chinese Acad Inspect & Quarantine, Inst Ind Prod Inspect, Beijing 100025, Peoples R China
来源：
CHROMATOGRAPHIA | 2010年 / 71卷 / 5-6期
关键词：
Gas chromatography-mass spectrometry; Ultrasonic nebulization extraction; Headspace single-drop microextraction; Essential oil; Zanthoxylum bungeanum Maxim; CHROMATOGRAPHY-MASS-SPECTROMETRY; GAS-CHROMATOGRAPHY; ASSISTED EXTRACTION; ESSENTIAL OILS; COMPONENTS; DISTILLATION;
D O I：
10.1365/s10337-010-1497-x
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
Ultrasonic nebulization extraction (UNE) combined with headspace single-drop microextraction (HS-SDME) and gas chromatography-mass spectrometry (GC-MS) have been used for rapid analysis of volatile components of the pericarp of Zanthoxylum bungeanum Maxim. Effective extraction was achieved by suspending 2 mu L n-heptadecane from the tip of a microsyringe, extracting for 15 min, and enriching for 25 min. The method combines the advantages of UNE and HS-SDME. Thirty-four compounds were identified in the pericarp of Zanthoxylum bungeanum Maxim. Compared with stirring extraction (SE)-HS-SDME and UNE, UNE-HS-SDME was resulted in higher extraction yield, enrichment efficiency, and sensitivity. The results indicate that UNE-HS-SDME is a feasible alternative method for analysis of essential oils from spices.
引用
收藏
页码：455 / 459
页数：5
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