A study on synthesis and properties of Fe3O4 nanoparticles by solvothermal method

被引:42
|
作者
Huang Yana [1 ]
Zhang Liping [1 ]
Huan Weiwei [1 ]
Liang Xiaojuan [2 ]
Liu Xiangnong [3 ]
Yang Yuxiang [1 ]
机构
[1] E China Univ Sci & Technol, Dept Chem, Shanghai 200237, Peoples R China
[2] Dalian Maritime Univ, Dalian 116021, Peoples R China
[3] Yangzhou Univ, Anal Test Ctr, Yangzhou 225009, Peoples R China
基金
中国国家自然科学基金;
关键词
Fe3O4; nanoparticles; solvothermal; magnetic properties; MAGNETITE NANOCRYSTALS; PARTICLES; SIZE; TEMPLATE; COLLOIDS;
D O I
10.1134/S1087659610030090
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Magnetic nanoparticles (Fe3O4) were synthesized by the solvothermal method using FeCl3 center dot 6H(2)O and ethylene glycol as a reactant. Powder X-ray diffraction, FT-IR, TEM, SEM, and VSM were used to characterize the magnetic particles. The reacting factors, such as reacting time, the concentration of iron source and surfactant, especially the effect of NaAc center dot 3H(2)O, were studied. The results indicated that NaAc center dot 3H(2)O plays the role not only as a dispersant but also a structure-directing agent. The synthesized Fe3O4 particles showed excellent magnetic property, which made them have potential for application in magnetic nanodevices and biomedicine.
引用
收藏
页码:325 / 331
页数:7
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