A study on synthesis and properties of Fe3O4 nanoparticles by solvothermal method

被引：42
|
作者：
Huang Yana [1 ]
Zhang Liping [1 ]
Huan Weiwei [1 ]
Liang Xiaojuan [2 ]
Liu Xiangnong [3 ]
Yang Yuxiang [1 ]
机构：
[1] E China Univ Sci & Technol, Dept Chem, Shanghai 200237, Peoples R China
[2] Dalian Maritime Univ, Dalian 116021, Peoples R China
[3] Yangzhou Univ, Anal Test Ctr, Yangzhou 225009, Peoples R China
来源：
GLASS PHYSICS AND CHEMISTRY | 2010年 / 36卷 / 03期
基金：
中国国家自然科学基金;
关键词：
Fe3O4; nanoparticles; solvothermal; magnetic properties; MAGNETITE NANOCRYSTALS; PARTICLES; SIZE; TEMPLATE; COLLOIDS;
D O I：
10.1134/S1087659610030090
中图分类号：
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
Magnetic nanoparticles (Fe3O4) were synthesized by the solvothermal method using FeCl3 center dot 6H(2)O and ethylene glycol as a reactant. Powder X-ray diffraction, FT-IR, TEM, SEM, and VSM were used to characterize the magnetic particles. The reacting factors, such as reacting time, the concentration of iron source and surfactant, especially the effect of NaAc center dot 3H(2)O, were studied. The results indicated that NaAc center dot 3H(2)O plays the role not only as a dispersant but also a structure-directing agent. The synthesized Fe3O4 particles showed excellent magnetic property, which made them have potential for application in magnetic nanodevices and biomedicine.
引用
收藏
页码：325 / 331
页数：7
相关论文
共 50 条
  • [1] A study on synthesis and properties of Fe3O4 nanoparticles by solvothermal method
    Yan Huang
    Liping Zhang
    Weiwei Huan
    Xiaojuan Liang
    Xiangnong Liu
    Yuxiang Yang
    Glass Physics and Chemistry, 2010, 36 : 325 - 331
  • [2] Synthesis and Characterization of Fe3O4 Nanoparticles Prepared by Solvothermal Method
    Liang, Yanxia
    Jiang, Li
    Xu, Shuting
    Ju, Wentao
    Tao, Zhu
    Yang, Yumeng
    Peng, Xiaoling
    Wei, Guoying
    JOURNAL OF MATERIALS ENGINEERING AND PERFORMANCE, 2024, 33 (13) : 6804 - 6815
  • [3] A Facile Solvothermal Synthesis of Octahedral Fe3O4 Nanoparticles
    Ooi, Frances
    DuChene, Joseph S.
    Qiu, Jingjing
    Graham, Jeremy O.
    Engelhard, Mark H.
    Cao, Guixin
    Gai, Zheng
    Wei, Wei David
    SMALL, 2015, 11 (22) : 2649 - 2653
  • [4] Synthesis of Monodispersed Fe3O4 Magnetite Nanoparticles by Ethylene Glycol Solvothermal Method
    Xu, Gang
    Zhang, Min
    Ou, Ping
    Zhang, Yi
    Han, Gaorong
    ADVANCES IN CHEMICAL, MATERIAL AND METALLURGICAL ENGINEERING, PTS 1-5, 2013, 634-638 : 2276 - 2279
  • [5] Solvothermal Synthesis and Magnetic Properties of Fe3O4 Microspheres
    Sun, Dehui
    Zhang, Jilin
    Sun, Dexin
    BIOTECHNOLOGY, CHEMICAL AND MATERIALS ENGINEERING, PTS 1-3, 2012, 393-395 : 947 - +
  • [6] Microwave-solvothermal synthesis of Fe3O4 magnetic nanoparticles
    Li, Cuiyan
    Wei, Yajun
    Liivat, Anti
    Zhu, Yihua
    Zhu, Jiefang
    MATERIALS LETTERS, 2013, 107 : 23 - 26
  • [7] Solvothermal synthesis of Sm3+-doped Fe3O4 nanoparticles
    Lastovina, T. A.
    Budnyk, A. P.
    Kudryavtsev, E. A.
    Nikoisky, A. V.
    Kozakov, A. T.
    Chumakov, N. K.
    Emelyanov, A. V.
    Soldatov, A. V.
    MATERIALS SCIENCE & ENGINEERING C-MATERIALS FOR BIOLOGICAL APPLICATIONS, 2017, 80 : 110 - 116
  • [8] Solvothermal synthesis of magnetic Fe3O4 microparticles via self-assembly of Fe3O4 nanoparticles
    Wei Zhang
    Particuology, 2011, 9 (02) : 179 - 186
  • [9] Solvothermal synthesis of magnetic Fe3O4 microparticles via self-assembly of Fe3O4 nanoparticles
    Zhang, Wei
    Shen, Fenglei
    Hong, Ruoyu
    PARTICUOLOGY, 2011, 9 (02) : 179 - 186
  • [10] Synthesis and Characterization of Co2+-doped Fe3O4 Nanoparticles by the Solvothermal Method
    Sun, Xuejiao
    Liu, Futian
    Jiang, Qinghui
    NANO-SCALE AND AMOURPHOUS MATERIALS, 2011, 688 : 364 - 369
12345