Fe3O4@SiO2-CPTMS-Guanidine-SO3H-catalyzed One-Pot Multicomponent Synthesis of Polysubstituted Pyrrole Derivatives under Solvent-Free Conditions

被引:15
|
作者
Rostami, H. [1 ]
Shiri, L. [1 ]
机构
[1] Ilam Univ, Fac Basic Sci, Dept Chem, Ilam, Iran
关键词
polysubstituted pyrrole derivatives; magnetic nanocatalyst; aniline derivatives; beta-diketones; beta-ketoesters; beta-nitrostyrenes; 4-COMPONENT SYNTHESIS; SUBSTITUTED PYRROLES; EFFICIENT; AMINES; AGENTS;
D O I
10.1134/S1070428019080207
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A highly efficient procedure for the one-pot synthesis of polysubstituted pyrrole derivatives by the reaction between of aniline derivatives, beta-diketones or beta-ketoesters, and beta-nitrostyrene derivatives in the presence of Fe3O4@SiO2-CPTMS-guanidine-SO3H as a reusable magnetic nanocatalyst is reported. The magnetic nanocatalyst was prepared and fully characterized by FTIR spectroscopy, scanning electron microscopy, energy dispersive X-ray spectroscopy, X-ray diffraction analysis, thermogravimetric analysis, and vibrating sample magnetometry.
引用
收藏
页码:1204 / 1211
页数:8
相关论文
共 50 条
  • [21] [HSO3-pmim][CH3SO3] Catalyzed One-Pot Protocol for the Synthesis of Coumarins Under Solvent-Free Conditions
    Song, S. J.
    Liu, W. H.
    Ma, J. J.
    Qi, J. M.
    ASIAN JOURNAL OF CHEMISTRY, 2012, 24 (10) : 4433 - 4435
  • [22] One-pot Synthesis of 3,4-Dihydropyrimidin-2 (1h) -ones Catalyzed by SO3H-Functionalized Mesopolymer under Solvent-free Conditions
    Xing, Rong
    Zhang, Tong
    Zhang, Yue
    ACTA POLYMERICA SINICA, 2014, (05): : 613 - 618
  • [23] Fe3O4 nanoparticles: a highly efficient and easily reusable catalyst for the one-pot synthesis of xanthene derivatives under solvent-free conditions
    Ghasemzadeh, Mohammad Ali
    Safaei-Ghomi, Javad
    Zahedi, Safura
    JOURNAL OF THE SERBIAN CHEMICAL SOCIETY, 2013, 78 (06) : 769 - 779
  • [24] Uncatalyzed, One-pot Synthesis of 3,3′-(Benzylene)-bis(4-hydroxy-2H-chromen-2-one) Derivatives under Thermal Solvent-free Conditions
    Shaterian, Hamid Reza
    Honarmand, Moones
    CHINESE JOURNAL OF CHEMISTRY, 2009, 27 (09) : 1795 - 1800
  • [25] Bronsted Acidic Ionic Liquid-Catalyzed One-Pot Synthesis of 4(3H)-Quinazolinones under Solvent-Free Conditions
    Chatterjee, Rana
    Sarkar, Subhankar
    Santra, Sougata
    Zyryanov, Grigory, V
    Majee, Adinath
    MODERN SYNTHETIC METHODOLOGIES FOR CREATING DRUGS AND FUNCTIONAL MATERIALS (MOSM2019), 2020, 2280
  • [26] Zinc perchlorate catalyzed one-pot synthesis of 3,4-dihydropyrimidinones under solvent-free conditions
    Palekar, Vikrant S.
    Shukla, Sanjeev R.
    GREEN CHEMISTRY LETTERS AND REVIEWS, 2008, 1 (03) : 185 - 190
  • [27] Ammonium chloride catalyzed one-pot diindolylmethanes under solvent-free synthesis of conditions
    Azizian, Javad
    Teimouri, Fatemeh
    Mohammadizadeh, Mohammad Reza
    CATALYSIS COMMUNICATIONS, 2007, 8 (07) : 1117 - 1121
  • [28] Green and Efficient One-Pot Synthesis of 2-Amino-3-phenylsulphonyl-4H-chromenes under Solvent-Free Conditions
    Yu Xiaomeng
    Hu Xiaoyun
    Zhou Zhongqiang
    IRANIAN JOURNAL OF CHEMISTRY & CHEMICAL ENGINEERING-INTERNATIONAL ENGLISH EDITION, 2018, 37 (05): : 31 - 38
  • [29] A facile solvent-free route for the one-pot multicomponent synthesis of benzylpyrazolyl coumarins catalyzed by FeCl3•SiO2 nanoparticles
    Piruzmand, Z.
    Safaei-Ghomi, J.
    Ghasemzadeh, M. A.
    BULGARIAN CHEMICAL COMMUNICATIONS, 2016, 48 (04): : 619 - 623
  • [30] Fe2O3 as an Environmentally Benign Natural Catalyst for One-Pot and Solvent-Free Synthesis of Spiro-4H-Pyran Derivatives
    Maghsoodlou, Malek Taher
    Heydari, Reza
    Mohamadpour, Farzaneh
    Lashkari, Mojtaba
    IRANIAN JOURNAL OF CHEMISTRY & CHEMICAL ENGINEERING-INTERNATIONAL ENGLISH EDITION, 2017, 36 (04): : 31 - 38