Synthesis and Structural Characterization of a Nickel Coordination Polymer Based on 4-(1H-Imidazol-1-yl)phenyl)methanone with Phthalic Acid

被引：0

作者：

Sun, Shu-Wen ^{[1
]}

Wang, Gao-Feng ^{[1
]}

Zhang, Xiao ^{[2
]}

机构：

[1] Yuncheng Univ, Dept Appl Chem, Yuncheng 044000, Peoples R China

[2] Harbin Inst Technol, Sch Chem & Chem Engn, MIIT Key Lab Crit Mat Technol New Energy Convers, Harbin 150080, Heilongjiang, Peoples R China

来源：

CRYSTALLOGRAPHY REPORTS | 2018年 / 63卷 / 07期

关键词：

CRYSTAL-STRUCTURES; DIVERSITY;

D O I：

10.1134/S1063774518070246

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

A nickel coordination polymer with V-shaped ligands, {[(L-1)(2)Ni(H2O)(2)] 2(C8H5O4)}(n), (L-1 = 4-(1H-imidazol-1-yl)phenyl)methanone) has been synthesized under the solvothermal conditions. The structure has been determined by the single-crystal X-ray diffraction analysis and characterized by the infrared spectroscopy and elemental analysis. The crystal is crystallized in the monoclinic sp. gr. P2(1)/c with the unit cell parameters a = 15.6387(3) angstrom, b = 8.0526(2) angstrom, c = 24.4791(6) angstrom, and = 129.2350(10)degrees, Z = 2. The adjacent [Ni(H2O)(2)] units are linked by two bridging L-1 ligands to form 1D looped chains, which are extended by the hydrogen bonds to yield a 3D framework.

引用

页码：1120 / 1123

页数：4

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