[1] Tech Univ Munich, Heinz Maier Leibnitz Zentrum MLZ, Lichtenbergstr 1, D-85748 Garching, Germany
[2] Helmholtz Zentrum Geesthacht, German Engn Mat Sci Ctr, Max Planck Str, D-21502 Geesthacht, Germany
[3] Ludwig Maximilians Univ Munchen, Dept Geo & Umweltwissensch, Theresienstr 41, D-80333 Munich, Germany
[4] Inst Laue Langevin, 71 Ave Martyrs, F-38042 Grenoble, France