Spark Plasma Sintering of Ultrafine TiCxN1-x Powders Synthesized by a Mechanically Induced Self-Sustaining Reaction

被引：11

作者：

Borrell, Amparo ^{[1
]}

Fernandez, Adolfo ^{[2
]}

Torrecillas, Ramon ^{[1
]}

Cordoba, Jose M. ^{[3
]}

Aviles, Miguel A. ^{[3
]}

Gotor, Francisco J. ^{[3
]}

机构：

[1] CSIC, CINN, Llanera 33428, Asturias, Spain

[2] Fdn ITMA, Llanera 33428, Asturias, Spain

[3] CSIC US, Inst Ciencia Mat Sevilla, Seville 41092, Spain

来源：

JOURNAL OF THE AMERICAN CERAMIC SOCIETY | 2010年 / 93卷 / 08期

关键词：

TITANIUM CARBONITRIDE PHASES; REDUCTION; TIO2;

D O I：

10.1111/j.1551-2916.2010.03735.x

中图分类号：

TQ174 [陶瓷工业]; TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

High-purity, nanometer-sized titanium carbonitride powders, TiCxN1-x, were obtained with a mechanically induced self-sustaining reaction (MSR) in a high-energy planetary ball mill from a mixture of titanium and different carbon precursors under a nitrogen atmosphere. A promising method for developing dense TiCxN1-x materials is the coupling of MSR with the spark plasma sintering (SPS) technique. The powders were sintered at different temperatures to provide a completely dense monolithic ceramic (> 99% theoretical density). In this work, the influence of the carbon precursor and SPS treatment on the material microstructures were studied, and the main mechanical properties of the end material were evaluated.

引用

页码：2252 / 2256

页数：5

共 42 条

[41] Enhanced "overall" ionic conductivity in Li1+xAlxTi2- x(PO4)3 (0.3 ≤ x ≤ 0.7) ceramics prepared from sol-gel powders by spark plasma sintering
Martinez-Chaparro, S.
Kobylianska, S.
Sobrados, I.
Jimenez, R.
Sanz, J.
[J]. JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2022, 42 (10) : 4248 - 4258
[42] High carrier concentration in Mg2Si1-xSbx (0 ≤ x ≤ 0.10) prepared by a combination of liquid-solid reaction, ball milling, and spark plasma sintering
Kato, Daisuke
Iwasaki, Kouta
Yoshino, Masahito
Yamada, Tomoaki
Nagasaki, Takanori
[J]. INTERMETALLICS, 2017, 81 : 47 - 51

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