Synthesis of Co3O4 nanorod bunches from a single precursor CO(CO3)0.35Cl0.20(OH)1.10

被引：59
|
作者：
Wang, ZH
Chen, XY
Zhang, M
Qian, YT [1 ]
机构：
[1] Univ Sci & Technol China, Struct Res Lab, Anhua 230026, Peoples R China
[2] Univ Sci & Technol China, Dept Chem, Anhua 230026, Peoples R China
来源：
SOLID STATE SCIENCES | 2005年 / 7卷 / 01期
基金：
中国国家自然科学基金;
关键词：
nanorod bunches; thermal decomposition; CO3O4; precursor;
D O I：
10.1016/j.solidstatesciences.2004.10.032
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
CO3O4 nanorods were successfully synthesized from a single precursor via a thermal decomposition and oxidization route. The precursor used was Co(CO3)(0.35)Cl-0.20(OH)(1.10), which was prepared by a hydrothermal reaction using CoCl2(.)6H(2)O with CO(NH2)(2) at 95-120degreesC. Both the precursor and the as-prepared Co3O4 were characterized with XRD, TEM, SEM, TGA and XPS. The precursor, as well as CO3O4, was found to be composed of nanorods that were radially bunched. The Co3O4 nanorods obtained through a thermal treatment at 300 degreesC for 5 h were found to have a porous structure. (C) 2004 Elsevier SAS. All rights reserved.
引用
收藏
页码：13 / 15
页数：3
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