Capillary electrophoretic determination of tetramethylthuram disulphide (Thiram)

被引:21
|
作者
Malik, AK [1 ]
Faubel, W [1 ]
机构
[1] Forschungszentrum Karlsruhe GmbH, Inst Instrumentalle Analyt, D-76021 Karlsruhe, Germany
关键词
Thiram; capillary electrophoresis; environmental samples; Nabam; wheat samples;
D O I
10.1080/00032710008543174
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A simple and sensitive capillary electrophoretic method was developed for the separation and determination of Thiram in boric acid buffer by direct UV absorbance detection at lambda = 254 nm. The separation behaviour of Thiram from Nabam was studied and it is dependent on pH and the nature of the buffer. The detection limit (S/N = 3) is 0.5 mu g/ml for Thiram, The method was successfully applied to the analysis of wheat samples spiked with Thiram.
引用
收藏
页码:2055 / 2064
页数:10
相关论文
共 50 条
  • [1] Simple and sensitive method for determination of tetramethylthiuram disulphide (thiram)
    Malik, AK
    Kaul, KN
    Lark, BS
    Rao, ALJ
    PESTICIDE SCIENCE, 1998, 53 (01): : 104 - 106
  • [2] Capillary electrophoretic determination of resveratrol in wines
    Gu, XL
    Creasy, L
    Kester, A
    Zeece, M
    JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1999, 47 (08) : 3223 - 3227
  • [3] Chromatographic and capillary electrophoretic determination of microcystins
    Trojanowicz, Marek
    JOURNAL OF SEPARATION SCIENCE, 2010, 33 (03) : 359 - 371
  • [4] Capillary electrophoretic determination of ions in soils
    Ahumada, I
    Schalscha, E
    Soto, R
    BOLETIN DE LA SOCIEDAD CHILENA DE QUIMICA, 1997, 42 (04): : 527 - 534
  • [5] Determination of estriol by capillary electrophoretic immunoassay
    Su, P
    Wang, YC
    Zang, XX
    Chang, WB
    CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2003, 31 (04) : 385 - 388
  • [6] Capillary electrophoretic determination of silicon in plants
    Nikonorov, V. V.
    Nikitina, T. G.
    MICROCHEMICAL JOURNAL, 2016, 127 : 7 - 10
  • [7] Capillary electrophoretic determination of oxalate in amniotic fluid
    Nelson, BC
    Rockwell, GF
    Campfield, T
    O'Grady, P
    Hernandez, RM
    Wise, SA
    ANALYTICA CHIMICA ACTA, 2000, 410 (1-2) : 1 - 10
  • [8] Capillary electrophoretic determination of dithiocarbamates and ethyl xanthate
    A. K. Malik
    W. Faubel
    Fresenius' Journal of Analytical Chemistry, 2000, 367 : 211 - 214
  • [9] Capillary electrophoretic determination of inorganic selenium species
    Dzierzgowska, M
    Pyrzyñska, K
    Pobozy, E
    JOURNAL OF CHROMATOGRAPHY A, 2003, 984 (02) : 291 - 295
  • [10] CAPILLARY ELECTROPHORETIC DETERMINATION OF THE COMPONENT MONOSACCHARIDES IN HEMICELLULOSES
    HUBER, C
    GRILL, E
    OEFNER, P
    BOBLETER, O
    FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 1994, 348 (12): : 825 - 831