Low temperature chemical synthesis of nanocrystalline Pb(Mg1/3Nb2/3)O3 and (1-x)Pb(Mg1/3Nb2/3)O3-xPb(Fe1/2Nb1/2)O3 (x=0.1, 0.2, and 1) ceramics

被引：2
|
作者：
Das, RN [1 ]
Ray, JC
Pramanik, P
机构：
[1] Indian Inst Technol, Dept Met Engn & Mat Sci, Bombay 400076, Maharashtra, India
[2] Indian Inst Technol, Dept Chem, Kharagpur 721302, W Bengal, India
来源：
JOURNAL OF MATERIALS RESEARCH | 2000年 / 15卷 / 11期
关键词：
D O I：
10.1557/JMR.2000.0324
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Nanocrystalline (20 nm) lead magnesium niobate (PMN) powders were prepared via a chemical process. This process involved the addition of aqueous niobium tartrate, lead-ethylenediaminetetraacetic acid, and magnesium-polyvinyl alcohol complex to produce a homogeneous solution. After the complete evaporation of the resulting homogeneous solution, the complexes decomposed and produced a black, fluffy precursor material. The precursor material on calcination up to 850 degreesC/2 h produced nanocrystalline PMN powders with the corresponding average particle size 20 nm. PMN powders modified with lead iron niobate (PFN) (1 - x)PMN-xPFN (x = 0.1, 0.2, and 1) were also prepared using this route and investigated through x-ray diffraction studies.
引用
收藏
页码：2273 / 2275
页数：3
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