Chemical Vapor Transport Growth of ZrSe2 Crystals Using Cl2 as a Transport Agent

被引：5
|
作者：
Nikonov, K. S. [1 ]
Brekhovskikh, M. N. [1 ]
Menshchikova, T. K. [1 ]
Fedorov, V. A. [1 ]
机构：
[1] Russian Acad Sci, Kurnakov Inst Gen & Inorgan Chem, Leninskii Pr 31, Moscow 119991, Russia
来源：
INORGANIC MATERIALS | 2019年 / 55卷 / 09期
关键词：
single crystals; growth; X-ray diffraction; transition metal dichalcogenides; ZrSe2; chemical vapor transport;
D O I：
10.1134/S0020168519090097
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
A process has been proposed for ZrSe2 crystal growth with the use of ZrOCl2 as a transport agent source. The crystals thus grown have been characterized by X-ray diffraction. It has been shown that, unlike in the case of vanadium and molybdenum diselenides, the use of zirconium chloride causes no increase in crystal size. A mechanism of the chemical vapor transport process involved is proposed.
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页码：898 / 902
页数：5
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