Preparation of Several Active N-Chloro Compounds from Trichloroisocyanuric Acid

被引：28
|
作者：
Shiri, Azam [1 ]
Khoramabadi-zad, Ahmad [1 ]
机构：
[1] Bu Ali Sina Univ, Fac Chem, Hamadan, Iran
来源：
SYNTHESIS-STUTTGART | 2009年 / 16期
关键词：
chlorinated compounds; imides; amides; halogenation; trichloroisocyanuric acid; MOLECULAR CLIPS; ENCAPSULATION; GLYCOLURIL; IODINATION; PROTEINS;
D O I：
10.1055/s-0029-1216889
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A very simple method for the preparation of several active N-chloro compounds that have extensive applications in organic synthesis, industry, and medicine has been developed. Tetrachloroglycolurils, chloramine-T, N-chlorosaccharin, N-chlorosuccinimide, N-chlorophthalimide, N,N'-dichlorophenobarbital, and N,N'-dichlorobarbital were synthesized by chlorination with trichloroisocyanuric acid under mild reaction conditions at room temperature. This method is clean, fast, and efficient; the yields are also good to excellent.
引用
收藏
页码：2797 / 2801
页数：5
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