Syntheses and characterizations of two new pillared-layer coordination polymers constructed from lanthanides and mixed O-donor ligands

被引：12

作者：

Lin, Xi ^{[1
]}

Liu, Tianfu ^{[1
]}

Lin, Jingxiang ^{[1
]}

Yang, Hongxun ^{[1
]}

Lue, Jian ^{[1
]}

Xu, Bo ^{[1
]}

Cao, Rong ^{[1
]}

机构：

[1] Chinese Acad Sci, Fujian Inst Res Struct Matter, State Key Lab Struct Chem, Fuzhou 350002, Fujian, Peoples R China

来源：

INORGANIC CHEMISTRY COMMUNICATIONS | 2010年 / 13卷 / 03期

关键词：

Lanthanide; Pillared-layer; Hydrothermal; Anti-ferromagnetic; METAL-ORGANIC FRAMEWORKS; SINGLE-MOLECULE MAGNETS; CRYSTAL-STRUCTURE; CLUSTERS; RELAXATION; COMPLEXES; BEHAVIOR; ACID; MOF;

D O I：

10.1016/j.inoche.2009.12.030

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Two new pillared-layer frameworks have been obtained through self-assembly of 4,4'-azobenzene dicarboxylatic acid (4,4'-H(2)ABDC), oxalate, hydroxyl and LnCl(3)(Ln = Sm, Eu) under hydrothermal environment and characterized by TGA. IR spectroscopy, element analyses, and X-ray single crystal diffraction The X-ray Structure analyses reveal that the oxalates link the Ln(III) to form metal layers, and 4,4'-ABDC ligands work as pillars to connect adjacent layers to further extend into 3D frameworks Their magnetic studies show that the two compounds have typical anti-ferromagnetic behaviors (C) 2010 Elsevier B V All rights reserved

引用

页码：388 / 391

页数：4

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