Microwave synthesis of Fe-SBA-16 mesoporous silica and Friedel-Crafts type reaction

被引：0
|
作者：
Han, Dae-Soo [1 ]
Sujandi [1 ]
Koo, Jeong-Boon [1 ]
Park, Sang-Eon [1 ]
机构：
[1] Inha Univ, Lab Nanogreen Catalysis, Nano Ctr Fine Chem Fus Technol, Dept Chem, Inchon 402751, South Korea
来源：
RECENT PROGRESS IN MESOSTRUCTURED MATERIALS, PROCEEDINGS OF THE 5TH INTERNATIONAL MESOSTRUCTURED MATERIALS SYMPOSIUM - IMMS2006 | 2007年 / 165卷
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D O I：
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中图分类号：
O69 [应用化学];
学科分类号：
081704 ;
摘要：
Iron-substituted SBA-16 materials have been synthesized by using direct microwave synthesis method under weak acidic conditions. Different iron species including isolated framework iron species, iron cluster and iron oxides were formed by adjusting the pH value and Si/Fe molar ratios. All the materials has been characterized by XRD, N-2 sorption and SEM. Lewis acid catalyzed Friedel-Crafts type alkylation reaction of benzene with benzylchloride has been investigated over Fe catalysts prepared with different pH values and iron contents.
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页码：659 / 662
页数：4
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