SYNTHESIS OF MCM-41 MESOPOROUS MATERIAL USING FRESHWATER SPONGE AS A SOURCE OF SILICA

被引:0
|
作者
Lacerda Junior, Orivaldo da Silva [1 ]
Cavalcanti, Rodrigo Marinho [1 ]
de Matos, Thaisa Moreira [1 ]
Venancio, Jocilandia de Brito [1 ]
de Barros, Iuri Bezerra [1 ]
da Veiga-Junior, Valdir Florencio [1 ]
Lopes Barros, Ivoneide de Carvalho [1 ]
机构
[1] Univ Fed Amazonas, Dept Quim, Inst Ciencias Exatas, BR-69077000 Manaus, Amazonas, Brazil
来源
QUIMICA NOVA | 2013年 / 36卷 / 09期
关键词
synthesis; bio-silica; mesoporous; AREA;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Fresh water sponge was used as a silica source for the synthesis of MCM-41 via the hydrothermal process. The silica was extracted from the sponge by washing with nitric acid and piranha solution. Synthesis of MCM-41 was performed at 100 degrees C for 5 days and the procedure was optimized, with modifications made to the leaching temperature of the silica and the synthesis of mesoporous material, which was characterized by XRD, FT-IR, SEM and adsorption of N-2. The optimal result was achieved at a temperature of 135 degrees C for 3 days, showing ordered mesoporous material with a surface area of 1080 m(2) g(-1).
引用
收藏
页码:1348 / 1353
页数:6
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