Development of Portable X-Ray Diffractometer Equipped with X-Ray Fluorescence Spectrometer and Its Application to Archaeology

被引:3
|
作者
Yamashita, Daisuke [1 ]
Ishizaki, Atsushi [1 ]
Uda, Masayuki [2 ]
机构
[1] Riken Keiki Co Ltd, Res Dept, Itabashi Ku, Tokyo 1748744, Japan
[2] Waseda Univ, Inst Nara Art, Nerima Ku, Tokyo 1790076, Japan
关键词
X-ray diffraction; X-ray fluorescence; portable; pigment; Tutankhamun; Egypt; archaeology; IDENTIFICATION; PIGMENTS; PIXE; FRESCOES; XRF;
D O I
10.2116/bunsekikagaku.58.347
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A portable X-ray diffractometer equipped with all X-ray fluorescence spectrometer was improved so as to obtain a diffraction pattern and a fluorescence Spectrum ill air from one and the same small area of a specimen. The reason why the portable XRD with all XRF spectrometer was specially designed for archaeology may be understood from the following facts : (1) some objects exhibited in museums are not allowed to be transferred from the open air to a vacuum, even if their volumes are small; (2) some objects are very difficult to move from their original sites; (3) some parts of exhibits are extremely fragile and cannot be examined in a vacuum; and (4) information on the chemical composition and structure from the same area of all object offers a better understanding of the constitutive materials of the object. Some examples of the use of a portable X-ray diffractometer equipped with all X-ray fluorescence spectrometer in the field are also introduced. Experimental results of Sho-kannon, Snew's mask and Tutankhamun's golden mask are shown here.
引用
收藏
页码:347 / 355
页数:9
相关论文
共 50 条
  • [22] A Low Energy X-Ray Fluorescence Spectrometer for Elemental Mapping X-Ray Microscopy
    Alberti, R.
    Longoni, A.
    Klatka, T.
    Guazzoni, C.
    Gianoncelli, A.
    Bacescu, D.
    Kaulich, B.
    [J]. 2008 IEEE NUCLEAR SCIENCE SYMPOSIUM AND MEDICAL IMAGING CONFERENCE (2008 NSS/MIC), VOLS 1-9, 2009, : 839 - +
  • [23] A high-resolution X-ray fluorescence spectrometer and its application at SSRF
    Gao, Xing
    Gu, Songqi
    Gao, Qian
    Zou, Yang
    Jiang, Zheng
    Zhang, Shuo
    Wei, Xiangjun
    Yu, Haisheng
    Sheng, Guodong
    Duan, Peiquan
    Huang, Yuying
    [J]. X-RAY SPECTROMETRY, 2013, 42 (06) : 502 - 507
  • [24] Hard x-ray spectrometer calibrations using a portable 120 kV x-ray source
    Seely, John F.
    [J]. REVIEW OF SCIENTIFIC INSTRUMENTS, 2022, 93 (09):
  • [25] Development and application of portable, hand-held X-ray fluorescence spectrometers
    Bosco, Gerra L.
    [J]. TRAC-TRENDS IN ANALYTICAL CHEMISTRY, 2013, 45 : 121 - 134
  • [26] ADJUSTING AN X-RAY DIFFRACTOMETER
    BONDARS, BY
    [J]. INDUSTRIAL LABORATORY, 1989, 55 (10): : 1151 - 1152
  • [27] DEVELOPMENT AND APPLICATION OF AN INSITU X-RAY FLUORESCENCE SPECTROMETER FOR UNDERWATER SEDIMENT ANALYSIS
    WOGMAN, NA
    NIELSON, KK
    [J]. ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1979, (APR): : 130 - &
  • [28] X-RAY DIFFRACTOMETER FURNACE
    WILCHINS.ZW
    TSIEN, HC
    VERSTRAT.G
    [J]. JOURNAL OF PHYSICS E-SCIENTIFIC INSTRUMENTS, 1971, 4 (SEP): : 704 - &
  • [29] MONOCHROMATIZATION ON THE X-RAY DIFFRACTOMETER
    BROLL, N
    [J]. ANALUSIS, 1983, 11 (01) : 36 - 41
  • [30] AN AUTOMATIC X-RAY DIFFRACTOMETER
    BROWN, PJ
    [J]. ACTA CRYSTALLOGRAPHICA, 1960, 13 (12): : 985 - 985