Single step polymerization of conducting poly(o-toluidine) doped with camphor sulphonic acid: Synthesis and characterization

被引:0
|
作者
Kulkarni, Milind V. [1 ]
Viswanath, Annamraju Kasi [1 ]
Khanna, P. K. [1 ]
机构
[1] Ctr Mat Elect Technol, Photon & Adv Mat Lab, Pune 411008, Maharashtra, India
关键词
polymers; chemical synthesis; spectroscopy; thermogravimetric analysis (TGA); conductivity;
D O I
暂无
中图分类号
O63 [高分子化学(高聚物)];
学科分类号
070305 ; 080501 ; 081704 ;
摘要
Single step chemical polymerization of o-toluidine was carried out by using ammonium persulphate as an oxidizing agent. This is a direct process to synthesize the conducting emeraldine salt phase of the polymer using camphor sulphonic acid as a dopant. The polymer was characterized by UV-Vis. and FT-IR spectroscopy, scanning electron microscopy, TGA/DSC, elemental analysis and conductivity measurements. This method offers a polymer having very good physico-chemical properties with good electrical conductivity.
引用
收藏
页码:487 / 498
页数:12
相关论文
共 50 条
  • [41] Synthesis and characterization of novel poly(o-toluidine) montmorillonite nanocomposites:: Effect of surfactant on intercalation
    Singhal, Rahul
    Datta, Monika
    JOURNAL OF APPLIED POLYMER SCIENCE, 2007, 106 (03) : 1909 - 1916
  • [42] Synthesis and characterization of poly(o-toluidine)/kaolinite conductive composites for humidity and temperature sensing
    Boran, Filiz
    Cetinkaya, Sevil
    Karakisla, Meral
    Sacak, Mehmet
    PAMUKKALE UNIVERSITY JOURNAL OF ENGINEERING SCIENCES-PAMUKKALE UNIVERSITESI MUHENDISLIK BILIMLERI DERGISI, 2018, 24 (07): : 1278 - 1283
  • [43] Carboxyl-functionalized MWCNT doped poly(o-toluidine) nanohybrids: Synthesis, characterization with AC electrical and dielectric properties
    Choudhury, Arup
    SYNTHETIC METALS, 2014, 188 : 13 - 20
  • [44] Electrochemical synthesis and electrochromic, photovoltaic properties of poly(o-toluidine)
    Niu, Hai-Jun
    Zhang, Mi-Lin
    Zang, Wen-Jing
    Zhang, Lin
    Bai, Xu-Duo
    Wang, Wen
    Cailiao Kexue yu Gongyi/Material Science and Technology, 2010, 18 (06): : 796 - 800
  • [45] Electrochemical and optical behaviour of poly(o-toluidine) conducting polymer in semisolid electrolytes
    Kumar, D
    Sharma, RC
    Ram, MK
    Dhawan, SK
    Chandra, S
    INDIAN JOURNAL OF CHEMISTRY SECTION A-INORGANIC BIO-INORGANIC PHYSICAL THEORETICAL & ANALYTICAL CHEMISTRY, 1997, 36 (01): : 14 - 18
  • [46] Conducting blends of poly(o-toluidine) and ethylene-propylene-diene terpolymer
    Ghosh, P
    Kar, SB
    Bhattacharyya, S
    JOURNAL OF APPLIED POLYMER SCIENCE, 2003, 88 (10) : 2550 - 2555
  • [47] A study on the electrochemical polymerization, characterization, and corrosion protection of o-toluidine on steel
    Vandana P. Shinde
    Pradip P. Patil
    Journal of Solid State Electrochemistry, 2013, 17 : 29 - 41
  • [48] O-toluidine Polymerization in Aqueous Phase and Its Development to Produce In Situ Poly-o-toluidine Films
    Asijati, Endang W.
    Susanto, Dieky
    Tockary, Theofilus A.
    Sabarinah, Yanti
    MAKARA JOURNAL OF SCIENCE, 2006, 10 (01) : 47 - +
  • [49] A study on the electrochemical polymerization, characterization, and corrosion protection of o-toluidine on steel
    Shinde, Vandana P.
    Patil, Pradip P.
    JOURNAL OF SOLID STATE ELECTROCHEMISTRY, 2013, 17 (01) : 29 - 41
  • [50] Synthesis and characterization of conducting homopolymers and copolymers of o-anisidine and o-toluidine in inorganic and organic supporting electrolytes
    Borole, DD
    Kapadi, UR
    Mahulikar, PP
    Hundiwale, DG
    JOURNAL OF APPLIED POLYMER SCIENCE, 2003, 90 (10) : 2634 - 2642