Synthesis and spectroscopic characterisation of LiFePO4 cathode materials

被引:0
|
作者
Lazarevic, Z. [1 ]
Krizan, G. [2 ,3 ]
Krizan, J. [4 ]
Mitric, M. [5 ]
Paunovic, N. [1 ]
Milutinovic, A. [1 ]
Romcevic, N. [1 ]
机构
[1] Univ Belgrade, Inst Phys, Pregrevica 118, Belgrade 11080, Serbia
[2] Natl Inst Chem, Dept Mat Chem, Ljubljana, Slovenia
[3] Univ Ljubljana, Fac Chem & Chem Technol, Ljubljana, Slovenia
[4] AMI Doo, Trstenjakova Ulica 5, Ptuj, Slovenia
[5] Univ Belgrade, Inst Nucl Sci Vinca, Belgrade, Serbia
关键词
Lithium iron phosphate; IR spectroscopy; Magnetic measurements; LITHIUM IRON PHOSPHATE; PULSE COMBUSTION REACTOR; TEMPERATURE;
D O I
暂无
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Lithium iron phosphate (LiFePO4) are synthesized in complete and incomplete combustion and calcined at 700 degrees C. The obtained samples were characterized by XRD, IR spectroscopy and magnetic measurement. Morphology of samples was controlled by SEM. The aim of this work is to show that it is possible to achieve a desired crystal phase by pulse combustion in a relatively cheap and fastway. The extremely rapid synthesis of almost pure phase material is possible due to the reduction in size of interacting particles and to an enormous number of collisions between them as a result of the strong turbulent flow associated with explosive combustion.
引用
收藏
页码:228 / 234
页数:7
相关论文
共 50 条
  • [21] Synthesis of LiFePO4 cathode material by microwave processing
    Higuchi, M
    Katayama, K
    Azuma, Y
    Yukawa, M
    Suhara, M
    JOURNAL OF POWER SOURCES, 2003, 119 : 258 - 261
  • [22] Sol-gel synthesis of LiFePO4 Cathode
    Hui Le
    Tang Zilong
    Luo Shaohua
    Zhang Zhongtai
    PROGRESS IN CHEMISTRY, 2007, 19 (10) : 1460 - 1466
  • [23] Design and Synthesis of In-situ VGCFs Improved LiFePO4 Composite Cathode Materials
    Deng, Fei
    Zeng, Xierong
    Zou, Jizhao
    Huang, Jianfeng
    Xiong, Xinbo
    Li, Xiaohua
    Sheng, Hongchao
    JOURNAL OF NEW MATERIALS FOR ELECTROCHEMICAL SYSTEMS, 2011, 14 (01) : 27 - 30
  • [24] Synthesis of LiFePO4 Cathode Materials by Mechanical-Activation-Assisted Polyol Processing
    Cao Yan-Bing
    Duan Jian-Guo
    Jiang Feng
    Hu Guo-Rong
    Peng Zhong-Dong
    Du Ke
    ACTA PHYSICO-CHIMICA SINICA, 2012, 28 (05) : 1183 - 1188
  • [25] Synthesis and Electrochemical Performance of LiFePO4/C Cathode Materials Using Fe Powder
    Meng Fang-Li
    Zhang Dong-Yun
    Chang Cheng-Kang
    Xu Jia-Yue
    Kamzin, A. S.
    JOURNAL OF INORGANIC MATERIALS, 2016, 31 (08) : 802 - 806
  • [26] Nanosized LiFePO4 Cathode materials for lithium ion batteries
    Gul, Hal-Bon
    Jun, Dae-Kyoo
    Park, Gye-Choon
    Jin, Bo
    Jin, En Mei
    JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, 2007, 7 (11) : 3980 - 3984
  • [27] Research Progress into the Structure and Performance of LiFePO4 Cathode Materials
    Hu Jiangtao
    Zheng Jiaxin
    Pan Feng
    ACTA PHYSICO-CHIMICA SINICA, 2019, 35 (04) : 361 - 370
  • [28] Synthesis and Characterization of LiFePO4/C Cathode Materials by Sol-Gel Method
    Liu, Shuxin
    Yin, Hengbo
    Wang, Haibin
    Wang, Hong
    JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, 2014, 14 (09) : 7060 - 7065
  • [29] Tunable Morphology Synthesis of LiFePO4 Nanoparticles as Cathode Materials for Lithium Ion Batteries
    Ma, Zhipeng
    Shao, Guangjie
    Fan, Yuqian
    Wang, Guiling
    Song, Jianjun
    Liu, Tingting
    ACS APPLIED MATERIALS & INTERFACES, 2014, 6 (12) : 9236 - 9244
  • [30] Synthesis and Electrochemical Characteristics of LiFePO4/C Cathode Materials from Different Precursors
    Gao, Jian
    Li, Jianjun
    He, Xiangming
    Jiang, Changyin
    Wan, Chunrong
    INTERNATIONAL JOURNAL OF ELECTROCHEMICAL SCIENCE, 2011, 6 (07): : 2818 - 2825