Synthesis of Nano-hydroxyapatite via Microbial Method and Its Characterization

被引:18
|
作者
Wang, Xin [1 ,2 ]
Qian, Chunxiang [1 ,2 ]
Yu, Xiaoniu [1 ,2 ]
机构
[1] Southeast Univ, Sch Mat Sci & Engn, Nanjing 211189, Jiangsu, Peoples R China
[2] Res Inst Green Construct Mat, Nanjing 211189, Jiangsu, Peoples R China
关键词
Microbial method; Hydroxyapatite; Mineralization; Nanoparticle; Characterization; IN-SITU; CARBONATED APATITE; THERMAL-STABILITY; POWDERS; TEMPERATURE; HYDROLYSIS; CERAMICS;
D O I
10.1007/s12010-014-0911-5
中图分类号
Q5 [生物化学]; Q7 [分子生物学];
学科分类号
071010 ; 081704 ;
摘要
Nanoparticles of hydroxyapatite were successfully synthesized by microbial method at ambient temperature and pressure, using calcium chloride and specific substrate as reactants. The compositional and morphological properties of products of the syntheses were studied by means of X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, scanning electron microscopy (SEM), transmission electron microscopy (TEM), and thermogravimetric analysis (TGA). The characterization data obtained showed that the phase composition, functional groups, and surface morphology of samples obtained by microbial method were mainly similar to that by chemical precipitation method. The hydroxyapatite powder was shown to be nanometer-grade in size and sphere-like in shape.
引用
收藏
页码:1003 / 1010
页数:8
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