Synthesis and Crystal Structure of 5-Methoxy-4′-chloro-2,2′-[ethylenedioxybis(nitrilomethylidyne)]diphenol

被引：0
|
作者：
Yang, Yu-Hua [1 ]
Zhang, Xin-Ying [1 ]
Zhao, Meng-Meng [1 ]
Li, Gang [1 ]
Dong, Xiu-Yan [1 ]
机构：
[1] Lanzhou Jiaotong Univ, Sch Chem & Biol Engn, Lanzhou 730070, Peoples R China
来源：
ASIAN JOURNAL OF CHEMISTRY | 2014年 / 26卷 / 04期
关键词：
Asymmetrical Salamo-type compound; Synthesis; Crystal structure; HYDROLYTIC KINETIC RESOLUTION; SCHIFF-BASE; COPPER(II) COMPLEXES; CO(SALEN) COMPLEXES; SPECTRAL PROPERTIES; MAGNETIC-PROPERTIES; BISOXIME LIGAND; SALEN; CATALYSTS;
D O I：
10.14233/ajchem.2014.16032
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
An asymmetrical Salamo-type compound 5-methoxy-4'-chloro-2,2'-[ethylenedioxybis(nitrilomethylidyne)]diphenol have been synthesized and characterized by single crystal X-ray crystallography. The crystal structure shows that the compound adopts an L-shaped configuration, in which the benzene rings are approximately perpendicular, making a dihedral angle of 84.09(3)degrees. And the molecule contains abundant intramolecular and intermolecular hydrogen bonding interactions. Thus, each molecule links six other molecules into an infinite 3D supramolecular structure by intermolecular hydrogen bonding interactions.
引用
收藏
页码：1133 / 1135
页数：3
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