Synthesis and Characterization of Novel Stilbene Derivatives with 1,3,4-Oxadiazole Unit

被引:5
|
作者
He, Dao-Hang [1 ]
Zhu, Yong-Chuang [1 ]
Yang, Zhuo-Ru [1 ]
Hu, Ai-Xi [2 ]
机构
[1] S China Univ Technol, Coll Chem & Chem Engn, Guangzhou 510640, Guangdong, Peoples R China
[2] Hunan Univ, Coll Chem & Chem Engn, Changsha 410082, Hunan, Peoples R China
关键词
Stilbene derivatives; 1,3,4-Oxadiazole unit; Synthesis; BACULOVIRUS; ENHANCERS; EMISSION; HOLE;
D O I
10.1002/jccs.200900039
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Four novel stilbene derivatives containing 1,3,4-oxadiazole unit have been synthesized in four steps with overall yields (27 similar to 35%). The synthetic route involved one-step installation of 2,5-di-p-tolyl-1,3,4-oxadiazol via the direct coupling of p-toluic acid with hydrazine hydrate promoted by PPA, benzylic bromination, conventional phosphonate formation, and Wittig-Horner olefination.
引用
收藏
页码:268 / 270
页数:3
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