The isomerization/chlorination of O,O-diallyl thiophosphoric(-nic) acid esters with phosphorus oxychloride - A new convenient method for synthesis of S-alkyl thiophosphoric(-nic) acid derivatives

被引：0

作者：

He, ZJ ^{[1
]}

Liu, JX ^{[1
]}

Zhou, ZH ^{[1
]}

Tang, CC ^{[1
]}

机构：

[1] Nankai Univ, State Key Lab Elementoorgan Chem, Tianjin 300071, Peoples R China

来源：

CHINESE CHEMICAL LETTERS | 1998年 / 9卷 / 10期

关键词：

isomerization; chlorination; phosphoro(-no)thionate; phosphoro(-no)thiolate; phosphoro(-no)chlorothiolate; phosphorus oxychloride;

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The isomerization/chlorination of O,O-diallyl thiophosphoric(-nic) acid esters with phosphrus oxychloride gives S-allyl thiophosphoro(-no)chloride, which reacts with substituted phenol in chloroform in the presence of triethylamine to afford eighteen new S-allyl thiophosphoric(-nic) acid derivatives. Thus, a new convenient method has been provided for synthesis of the title compounds.

引用

页码：903 / 905

页数：3

共 11 条

[1] The Isomerization/Chlorination of O,O-Diallyl Thiophosphoric (-nic) Acid Esters with Phosphorus Oxychloride─A New Convenient Method for Synthesis of S-Alkyl Thiophosphoric(-nic) Acid Derivatives
Zheng Jie HE
Ju Xiang LIU
Zheng Hong ZHOU
and Chu Chi TANG(State Key Laboratory of Elemento-Organic Chemistry
[J]. Chinese Chemical Letters, 1998, (10) : 903 - 905
[2] The chlorination reaction of O-alkyl S-alkyl(aryl) thiophosphoric(-nic) acid derivatives with phosphorus oxychloride
He, ZJ
Chen, WB
Ma, FP
Zhou, ZH
Tang, CC
[J]. PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 1998, 142 : 49 - 55
[3] The chlorination of O-alkyl S-alkyl(aryl) thiophosphoric(-nic) acids derivatives with phosphorus oxychloride -: A new method for synthesis of S-alkyl(aryl) thiophosphoro(-no)chloridates
He, ZJ
Chen, WB
Ma, FP
Zhou, ZH
Tang, CC
[J]. CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE, 1999, 20 (01): : 54 - 58
[4] The isomerization chlorination of O,O-dialkyl methylthiophosphonates with phosphorus oxychloride - A new convenient synthesis of S-alkyl methylthiophosphonic acid derivatives
Tang, CC
Ma, FP
Zhang, K
He, ZJ
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[5] A CONVENIENT SYNTHESIS OF S-ALKYL O-ARYL THIOPHOSPHORIC ACID-DERIVATIVES
TANG, CC
WU, GP
ZHANG, GZ
[J]. SYNTHESIS-STUTTGART, 1991, (06): : 454 - 456
[6] Studies on the synthesis of S-alkyl-O-polychlorophenyl thiophosphoric(-nic) acid derivatives and their fungicidal activities
Tang, CC
Jin, GY
Huang, GY
Ma, FP
Wu, GP
He, ZJ
Li, SZ
Li, BW
Zhang, SH
[J]. CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE, 1996, 17 (03): : 414 - 418
[7] The isomerization/chlorination of nitrogen heterocyclic O,O-dialkyl thiophosphoramidates with phosphorus oxychloride - A convenient synthesis of nitrogen heterocyclic S-alkyl thiophosphoramidic acid derivatives
Tang, CC
Lang, HF
He, ZJ
[J]. HETEROATOM CHEMISTRY, 1996, 7 (03) : 207 - 210
[8] THE ISOMERIZATION CHLORINATION OF O,O-DIALKYL-PHENYLTHIOPHOSPHONATES WITH PHOSPHORUS OXYCHLORIDE - A NEW CONVENIENT SYNTHESIS OF S-ALKYL-PHENYLTHIOPHOSPHONIC ACID-DERIVATIVES
TANG, CC
WU, GP
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LI, Z
JIN, GY
[J]. PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 1993, 84 (1-4): : 159 - 164
[9] The isomerization/chlorination of O,O-dialkyl N,N-dialkyl thiophosphoramidate with phosphorus oxychloride - A new method for synthesis of S-alkyl N,N-dialkyl thiophosphoramidic acid derivatives
Tang, CC
Wu, GP
He, SJ
He, ZJ
[J]. PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 1995, 101 (1-4): : 91 - 94
[10] A NEW CONVENIENT SYNTHESIS OF S-ALKYL N,N-DIALKYL THIOPHOSPHORAMIDIC ACID DERIVATIVES
Chu Chi TANG Gui Ping WU Institute of Elemento-Organic Chemistry
[J]. Chinese Chemical Letters, 1992, (08) : 593 - 594

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