Synthesis of 4'-[3-methyl-5-thioxo-1H-1,2,4-triazol-4(5H)-yl]-2',5'-diphenyl-2',4'-dihydro spiro[indolin-3,3'[1,2,4]triazol]-2-one derivatives

被引：14
|
作者：
Bazian, Atiye [1 ]
Taheri, Milad [1 ]
Alavi, Haniyeh [1 ]
机构：
[1] Islamic Azad Univ, Shahre Rey Branch, Dept Chem, Tehran, Iran
来源：
RUSSIAN JOURNAL OF GENERAL CHEMISTRY | 2014年 / 84卷 / 03期
关键词：
HYDRAZIDOYL HALIDES; 4-AMINO-4,5-DIHYDRO-1H-1,2,4-TRIAZOLE-5-ONES; DEHYDROCHLORINATION; NITRILIMINES; HETEROCYCLES; MECHANISM; KINETICS;
D O I：
10.1134/S107036321403030X
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
In this paper 1,3-dipolar cycloaddition reaction has been studied. An efficient synthesis of 4'-[3-methyl-5-thioxo-1H-1,2,4-triazol-4(5H)-yl]-2',5'-diphenyl-2',4'-dihydro spiro(indolin-3,3'[1,2,4]triazol)-2-one derivatives using triethylamine in MeCN at room temperature is reported. The structures of the obtained compounds were confirmed by means of elemental analysis, MS and spectral (IR, H-1, and C-13 NMR) methods.
引用
收藏
页码：586 / 592
页数：7
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