Determination of procaine hydrochloride by ion-pairing flow injection analysis with piezoelectric detection

被引：8
|
作者：
Mo, ZH [1 ]
Luo, J [1 ]
Long, XH [1 ]
Xia, ZL [1 ]
机构：
[1] CHONGQING UNIV,COLL CHEM & CHEM ENGN,CHONGQING 630044,PEOPLES R CHINA
来源：
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1997年 / 358卷 / 04期
关键词：
D O I：
10.1007/s002160050469
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A fast and simple method for the determination of procaine hydrochloride by ion-pairing flow injection analysis has been developed. It is based on the formation of an ion-pair with sodium dodecyl phenylsulphonate and piezoelectric detection. The calibration curve was linear between 0.02 and 2.00 mg/mL, with a detection limit of 0.01 mg/mL, a relative standard deviation of 0.3% (10 replicates) and a sampling frequency of 120/h. The proposed method has been satisfactorily applied to the determination of procaine hydrochloride in pharmaceutical preparations.
引用
收藏
页码：556 / 558
页数：3
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