Determination of multiclass pesticide residues in apple juice by gas chromatography-mass spectrometry with large-volume injection

被引：29

作者：

Wang, Jian-Hua ^{[1
]}

Zhang, Yi-Bing ^{[1
]}

Wang, Xiu-Lin ^{[1
]}

机构：

[1] Shandong Exit & Entry Inspect & Quarantine Bur, Shandong, Peoples R China

来源：

JOURNAL OF SEPARATION SCIENCE | 2006年 / 29卷 / 15期

关键词：

apple juice; large-volume injection programmed-temperature vaporizer injection; GC-MS; pesticide residue analysis;

D O I：

10.1002/jssc.200500250

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

This study presents two GC-MS SIM methods, in combination with large-volume injection programmed-temperature vaporization (LVI-PTV) injection, for the determination of 141 pesticide residues in apple juice. The sample was extracted with ACN, and coextractives were removed with primary/secondary amine sorbent. ACN extract (20 mu L) Was injected into a PTV injection port in solvent vent mode, and the pesticides were determined by GC-MS using retention time locking software. Deuterium-labeled pesticides (surrogate standards) were used for analytical quality control. In the validation experiments, pesticides recoveries were found to be 70-121% with RSDs of 4.6-21% (n = 6).

引用

页码：2330 / 2337

页数：8

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