Catalyst-free and solvent-free synthesis of novel symmetrical bisthioglycolic acid derivatives

被引：7
|
作者：
Pooladian, Baharak [1 ]
Ghasemi, Ehsan [1 ]
Karimi-Jaberi, Zahed [1 ]
机构：
[1] Islamic Azad Univ, Firoozabad Branch, Dept Chem, Firoozabad, Iran
来源：
GREEN CHEMISTRY LETTERS AND REVIEWS | 2014年 / 7卷 / 01期
关键词：
thioglycolic acid; catalyst-free; solvent-free; thioethers; aldehydes; EFFICIENT; 1,3-OXATHIOLAN-5-ONE; MILD;
D O I：
10.1080/17518253.2014.895861
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A simple, efficient, eco-friendly, and cost-effective method has been developed for the synthesis of symmetrical bisthioglycolic acid derivatives by a one-pot reaction of aldehydes or ketones with thioglycolic acid under solvent- and catalyst-free conditions in excellent yields (87-97%). The advantages of this novel protocol include the excellent yields, operational simplicity, short reaction times, and the avoidance of the use of organic solvents and catalysts.
引用
收藏
页码：60 / 63
页数：4
相关论文
共 50 条
  • [1] Green and catalyst-free synthesis of aminoanthraquinone derivatives in solvent-free conditions
    Sardashti-Birjandi, Arezoo
    Mollashahi, Ebrahim
    Maghsoodlou, Malek Taher
    Yazdani-Elah-Abadi, Afshin
    [J]. RESEARCH ON CHEMICAL INTERMEDIATES, 2021, 47 (09) : 3597 - 3608
  • [2] Green and catalyst-free synthesis of aminoanthraquinone derivatives in solvent-free conditions
    Arezoo Sardashti-Birjandi
    Ebrahim Mollashahi
    Malek Taher Maghsoodlou
    Afshin Yazdani-Elah-Abadi
    [J]. Research on Chemical Intermediates, 2021, 47 : 3597 - 3608
  • [3] Catalyst-free and solvent-free hydroboration of ketones
    Wang, Weifan
    Luo, Man
    Yao, Weiwei
    Ma, Mengtao
    Pullarkat, Sumod A.
    Xu, Li
    Leung, Pak-Hing
    [J]. NEW JOURNAL OF CHEMISTRY, 2019, 43 (27) : 10744 - 10749
  • [4] Catalyst-free and solvent-free hydroboration of aldehydes
    Stachowiak, Hanna
    Kazmierczak, Joanna
    Kucinski, Krzysztof
    Hreczycho, Grzegorz
    [J]. GREEN CHEMISTRY, 2018, 20 (08) : 1738 - 1742
  • [5] Catalyst-free and solvent-free hydroboration of alkynes
    Jaladi, Ashok Kumar
    Choi, Hyeon Seong
    An, Duk Keun
    [J]. NEW JOURNAL OF CHEMISTRY, 2020, 44 (32) : 13626 - 13632
  • [6] Rapid and efficient synthesis of formamidines in a catalyst-free and solvent-free system
    Zhou, Zitong
    Zhao, Yu
    Zhou, Donghua
    Li, Li
    Luo, Hui
    Cui, Liao
    Yang, Weiguang
    [J]. RSC ADVANCES, 2021, 11 (54) : 33868 - 33871
  • [7] Mixing with microwaves: solvent-free and catalyst-free synthesis of pyrazoles and diazepines
    Vaddula, Buchi Reddy
    Varma, Rajender S.
    Leazer, John
    [J]. TETRAHEDRON LETTERS, 2013, 54 (12) : 1538 - 1541
  • [8] Solvent-free and catalyst-free direct alkylation of alkenes
    Li, Meng-Yao
    Li, Jiatong
    Gu, Ao
    Nong, Xiao-Mei
    Zhai, Shuyang
    Yue, Zhu-Ying
    Feng, Chen-Guo
    Liu, Yingbin
    Lin, Guo-Qiang
    [J]. GREEN CHEMISTRY, 2023, 25 (18) : 7073 - 7078
  • [9] Catalyst-Free and Solvent-Free Facile Hydroboration of Imines
    Pandey, Vipin K.
    Donthireddy, Siva Nagendra Reddy
    Rit, Arnab
    [J]. CHEMISTRY-AN ASIAN JOURNAL, 2019, 14 (19) : 3255 - 3258
  • [10] Catalyst-free and solvent-free method for the synthesis of quinoxalines under microwave irradiation
    Zhou, Jian Feng
    Gong, Gui Xia
    Shi, Kun Bao
    Zhi, San Jun
    [J]. CHINESE CHEMICAL LETTERS, 2009, 20 (06) : 672 - 675
12345