1,3-bis(4-chlorophenyl)thiourea

被引:5
|
作者
Qin, Yong-Qi [1 ]
Jian, Fang-Fang [1 ]
Liang, Tong-Ling [1 ]
机构
[1] Qingdao Univ Sci & Technol, New Mat & Funct Coordinat Chem Lab, Qingdao 266042, Peoples R China
关键词
D O I
10.1107/S1600536806040499
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C13H10N2SCl2 was prepared by the reaction of p-chloroaniline, KOH and 4-chloro-1-isothiocyanatobenzene in ethanol solution at room temperature. The structure of the title compound is symmetrical. The molecule lies across a mirror plane. There are some weak C-H center dot center dot center dot S intermolecular interactions in the crystal structure.
引用
收藏
页码:O5043 / O5044
页数:2
相关论文
共 50 条
  • [41] 1-(4-chlorophenyl)-3-(2,6-dichlorobenzoyl)-thiourea
    Rauf, M. Khawar
    Badshah, Amin
    Bolte, Michael
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O3859 - O3861
  • [42] 1-(4-Chlorophenyl)-3-(2,4-dichlorobenzoyl)thiourea
    Rauf, M. Khawar
    Bolte, Michael
    Badshah, Amin
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O260 - U1596
  • [43] 1,3-bis(4-nitrophenyl)triazene
    Hörner, M
    Bresolin, L
    Bordinhao, J
    Hartmann, E
    Strähle, J
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 2003, 59 : O426 - O427
  • [44] [2-(4-Chlorophenyl)-1,3-selenazol-4-yl]methanol
    Cui, Jichun
    Li, Chuan
    Qiao, Yanling
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O3458 - +
  • [45] Diverse Mechanical Properties of 1,3-Bis(4-nitrophenyl) thiourea-DMSO Dimorphic Solvates
    Hasija, Avantika
    Bhandary, Subhrajyoti
    Mangalampalli, S. R. N. Kiran
    Chopra, Deepak
    CRYSTAL GROWTH & DESIGN, 2022, 22 (04) : 2058 - 2065
  • [46] 4-(4-Chlorophenyl)-2-(trichloromethylsulfanyl)1,3-thiazole
    Hartung, J
    Schmidt, P
    Svoboda, I
    Fuess, H
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O1736 - O1737
  • [47] N-(Biphenyl-4-carbonyl)-N′-(4-chlorophenyl)thiourea
    Yamin, Bohari M.
    Arif, M. Asyikin M.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O104 - U3429
  • [48] Bis(4-chlorophenyl)(5-pyrimidinyl)methanol
    Caruso, Francesco
    Rossi, Miriam
    Acta Crystallographica, Section C: Crystal Structure Communications, 1998, 54 (pt 11): : 1668 - 1670
  • [49] Bis(4-chlorophenyl)(5-pyrimidinyl)methanol
    Caruso, F
    Rossi, M
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1998, 54 : 1668 - 1670
  • [50] (+)-(S,S)-1,3-Bis[(tetrahydrofuran-2-yl)methyl]thiourea
    Pena, Ulises
    Bernes, Sylvain
    Gutierrez, Rene
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O96 - U2104