Dimephosphone analogs: II. Dialkyl(diaryl)-(2-methyl-4-oxopent-2-yl)phosphine Oxide Oximes: Synthesis, Structure, and Generation of Iminoxyl Radicals

被引：4

作者：

Tatarinov, D. A. ^{[1
]}

Mironov, V. F. ^{[1
]}

Kostin, A. A. ^{[1
]}

Mironova, E. V. ^{[1
]}

Krivolapov, D. B. ^{[1
]}

Morozov, V. I. ^{[1
]}

Nabiullin, V. N. ^{[1
]}

Il'yasov, A. V. ^{[1
]}

Buzykin, B. I. ^{[1
]}

机构：

[1] Russian Acad Sci, Arbuzov Inst Organ & Phys Chem, Kazan Sci Ctr, Kazan 420088, Tatarstan, Russia

来源：

RUSSIAN JOURNAL OF GENERAL CHEMISTRY | 2014年 / 84卷 / 05期

基金：

俄罗斯基础研究基金会;

关键词：

PARAMAGNETIC-RESONANCE SPECTROSCOPY; 2-OXIDE;

D O I：

10.1134/S107036321405020X

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Dialkyl(diaryl)-(2-methyl-4-oxopent-2-yl)phosphine oxide oximes have been synthesized for the first time. According to the X-ray diffraction data, these compounds in crystal exist as a single E isomer. Their structure in solution and the E/Z isomer ratio were determined by H-1 and C-13 NMR spectroscopy.

引用

页码：901 / 910

页数：10

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