Reaction of N-(3,3,3-trifluoro-2-trifluoromethylprop-1-enyl)dimethylamine with MgSO4 center dot 7H(2)O. Synthesis of 4,4-difluoro-5-trifluoromethyl2-(2,2,2-trifluoro-1-trifluoromethylethyl)-4H-1,3-dioxine and cis/trans-3-dimethylamino-2-trifluoromethacryloyl fluoride

被引：8

作者：

Popov, AV

Pushin, AN

Luzina, EL

机构：

[1] Inst. Physiologically Active S., Russian Academy of Sciences

来源：

RUSSIAN CHEMICAL BULLETIN | 1997年 / 46卷 / 05期

关键词：

polyfluorinated enamines, hydrolysis 4,4-difluoro-5-trifluoromethyl-2-(2,2,2-trifluoro-1-trifluoromethylethyl)-4H-1,3-dioxine, formation, decomposition; 3-dimethylamino-2-trifluoromethylacryloyl fluoride; 3,3,3-trifluoropropanal;

D O I：

10.1007/BF02496143

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

4,4-Difluoro-5-trifluoromethyl-2-(2,2,2-trifluoro-1-trifluoromethylethyl)-4H-1,3-dioxine and cis/trans-3-dimethylamino-2-trifluoromethacryloyl fluoride were obtained by reaction of N-(3,3,3-trifluoro-2-trifluoromethylprop-1-enyl)dimethylamine with MgSO4 . 7H(2)O.

引用

页码：1032 / 1033

页数：2

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