Reaction of N-(3,3,3-trifluoro-2-trifluoromethylprop-1-enyl)dimethylamine with MgSO4 center dot 7H(2)O. Synthesis of 4,4-difluoro-5-trifluoromethyl2-(2,2,2-trifluoro-1-trifluoromethylethyl)-4H-1,3-dioxine and cis/trans-3-dimethylamino-2-trifluoromethacryloyl fluoride

被引：8
|
作者：
Popov, AV
Pushin, AN
Luzina, EL
机构：
[1] Inst. Physiologically Active S., Russian Academy of Sciences
来源：
RUSSIAN CHEMICAL BULLETIN | 1997年 / 46卷 / 05期
关键词：
polyfluorinated enamines, hydrolysis 4,4-difluoro-5-trifluoromethyl-2-(2,2,2-trifluoro-1-trifluoromethylethyl)-4H-1,3-dioxine, formation, decomposition; 3-dimethylamino-2-trifluoromethylacryloyl fluoride; 3,3,3-trifluoropropanal;
D O I：
10.1007/BF02496143
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
4,4-Difluoro-5-trifluoromethyl-2-(2,2,2-trifluoro-1-trifluoromethylethyl)-4H-1,3-dioxine and cis/trans-3-dimethylamino-2-trifluoromethacryloyl fluoride were obtained by reaction of N-(3,3,3-trifluoro-2-trifluoromethylprop-1-enyl)dimethylamine with MgSO4 . 7H(2)O.
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页码：1032 / 1033
页数：2
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