Synthesis, crystal structure and magnetic properties of 2D bi-layered coordination polymer

被引：5
|
作者：
Han, Zhengbo [1 ]
Li, Juan
Gao, Jingqun
机构：
[1] Liaoning Univ, Sch Chem Sci & Engn, Shenyang 110036, Peoples R China
[2] Jilin Univ, Sch Publ Hlth, Changchun 130021, Peoples R China
来源：
JOURNAL OF COORDINATION CHEMISTRY | 2006年 / 59卷 / 14期
关键词：
nickel; pyridine-3,4-dicarboxylic acid; crystal structure; coordination polymer; magnetic properties;
D O I：
10.1080/00958970500537887
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A new coordination polymer, [Ni(pydc)(H2O)(2)] center dot H2O ( 1) (H(2)pydc = pyridine-3,4-dicarboxylic acid), have been synthesized by treating Ni(II) nitrate with 3,4-pyridinedicarboxylic acid under hydrothermal conditions. The single-crystal X-ray structure reveals that 1 is a 2D bi-layered coordination polymer. Single-crystals are triclinic, space group P (1) over bar, with a = 7.065(3), b = 7.812( 4), c = 9.031( 4) angstrom, alpha = 75.568(8), beta = 68.970( 8), gamma = 75.927(8) degrees, V = 444.0(3) angstrom(3), Z = 2. Variable temperature magnetic susceptibility measurements demonstrate a ferromagnetic interaction in 1.
引用
收藏
页码：1641 / 1647
页数：7
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