Solid-state and solution conformations of eleutherobin obtained from X-ray diffraction analysis and solution NOE data

被引：2
|
作者：
Cinel, B
Patrick, BO
Roberge, M
Andersen, RJ
机构：
[1] Univ British Columbia, Dept Chem, Vancouver, BC V6T 1Z1, Canada
[2] Univ British Columbia, Dept Earth & Ocean Sci, Vancouver, BC V6T 1Z1, Canada
[3] Univ British Columbia, Dept Biochem & Mol Biol, Vancouver, BC V6T 1Z3, Canada
来源：
TETRAHEDRON LETTERS | 2000年 / 41卷 / 16期
基金：
加拿大自然科学与工程研究理事会;
关键词：
D O I：
10.1016/S0040-4039(00)00269-0
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Single crystal X-ray diffraction analysis has revealed the solid-state conformation of the microtubule-stabilizing diterpenoid eleutherobin (1). NOE data obtained for 1 in CDCl3 and DMSO-d(6) are consistent with solution conformations that are virtually identical to the solid state conformation. (C) 2000 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码：2811 / 2815
页数：5
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