Production of Oil-in-Water Emulsions with Varying Dispersed-Phase Content using Confined Impinging Jet Mixers

被引:7
|
作者
Tripodi, Ernesto [1 ]
Lazidis, Aristodimos [1 ]
Norton, Ian T. [1 ]
Spyropoulos, Fotis [1 ]
机构
[1] Univ Birmingham, Sch Chem Engn, Birmingham B15 2TT, W Midlands, England
基金
英国工程与自然科学研究理事会;
关键词
MEAN DROP SIZE; ENERGY-DISSIPATION; EMULSIFICATION; COALESCENCE; HOMOGENIZER; TURBULENCE; BREAKUP; FLOW;
D O I
10.1021/acs.iecr.9b00634
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
This work reports for the first time on the use of Confined Impinging Jet Mixers (CIJM) for the production of emulsions with dispersed-phase content up to 80 wt %, in both the surfactant-poor and -rich regimes, following the exposure to varying CIJM hydrodynamic conditions. It was observed computationally and experimentally that the CIJM capacity resulted strictly dependent on the mass jet flow rate (W-jet > 176 g/min) and the pre-emulsion droplet size (>10 mu m). CIJM emulsification performance remained (almost) unaffected by the variation in the oil mass fraction. All systems showed the lowest droplet size (similar to 8 mu m) and similar droplet size distributions under the highest W-jet. Conditionally onto the Tween20 availability, the emulsion d(3)(,2) was primarily determined by formulation characteristics in the surfactant poor-regime and by the CIJM energy dissipation rate in the surfactant-rich regime. In conclusion, this study offers further insights into the CIJM suitability as a realistic alternative to already-established emulsification methods.
引用
收藏
页码:14859 / 14872
页数:14
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